为研究碳纳米管填充和负载的可控制备,通过沉积负载方法和湿化学填充法制备了不同负载率和填充率的碳纳米管,采用红外光谱仪、X射线衍射仪、高分辨透射电子显微镜和热重分析仪进行了结构表征分析.研究结果表明,负载率和填充率与C和Fe的比例有关.当C与Fe的质量比为4:1或8:1时,负载率分别为28.52%或16.17%,填充率分别为11.32%或9.43%.
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