采用刷涂热分解法制备了Ti/Sb-SnO2电极,采用扫描电子显微镜(SEM)、能量色散谱(EDS)、X射线衍射仪(XRD)和电化学测量技术(包括线性扫描伏安曲线、循环伏安曲线和计时电位曲线)对所制备电极的微观形貌、元素组成、物相组成和电化学性能进行了分析.结果表明:Ti基体表面为蜂窝状结构,而Ti/Sb-SnO2电极表面形成了SnO2晶胞,电极表面活性层的催化性能明显提高.
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