欢迎登录材料期刊网

材料期刊网

高级检索

将自制的25 kg级BaZrO3坩埚用于Ti-55.8%Ni合金(质量分数)的真空感应熔炼,并将合金铸锭经锻造、轧制、拉拔等工序制成φ1.0 mm的TiNi合金丝材,取样经不同的制度热处理后,分析了TiNi合金丝材的拉伸性能、低周弯曲疲劳性能以及拉伸、疲劳断口形貌。结果表明:丝材经700℃保温1 h水淬处理后,延伸率可达23%,韧窝尺寸变小、数量增多,且微孔数量大幅减少。此外,丝材经500℃或550℃保温20 min水淬处理后,疲劳寿命得到提高,最高可达3072次,疲劳断口处贝纹线排列紧密,裂纹较短且部分存在分叉现象。

Ti-55.8 wt%Ni alloy ingot was prepared by vacuum induction melting in 25 kg-grade home-made BaZrO 3 crucible, and the ingot was turned into φ1.0 mm wire by forging, rolling, drawing and etc.For the TiNi wire samples followed by different heat treatments , their tensile properties , low cyclic bending fatigue behaviors , fractographies and fatigue fractography morphologies were analyzed .The results show that , after water quenching at 700 ℃for 1 h, the elongation of samples can reach 23%, and the sizes of dimples become smaller , while the numbers of dimples and micropores are shrink.Besides, after water quenching at 500 ℃ or 550 ℃ for 20 min, the fatigue life of samples is improved, which can reach 3 072 times.Cowrie pattern lines of fatigue fractographies are arrayed closely , and cracks in the matrix are small and part of the cracks are bifurcate .

参考文献

[1] 国子明,朱明,高永辉,毛协民,鲁雄刚,李重河.TiNi合金制备技术及连续铸造的可行性探讨[J].钛工业进展,2009(02):19-23.
[2] 刘礼华;杨恒;王利明.镍钛形状记忆合金应用及产业化现状[J].新材料产业,2002(8):29-32.
[3] 贺志荣,王芳,周敬恩.TiNi合金的超弹性及其工程应用研究进展[J].钛工业进展,2005(02):10-16.
[4] 冯昭伟,千东范,高宝东,刘雅秀,王江波.TiNiZr 形状记忆合金的性能研究[J].稀有金属,2001(01):47-50.
[5] 张文娟,朱明,冯景苏.NiTi合金腐蚀性能研究[J].稀有金属,2003(06):714-717.
[6] 曹继敏,杨冠军,邓炬.钛镍合金的研究开发及市场状况[J].钛工业进展,2002(05):4-8.
[7] K. Matsugi;H. Mamiya;Y. B. Choi;G. Sasaki;O. Yanagisawa;H. Kuramoto .Melting and solidification of TiNi alloys by cold crucible levitation method and evaluation of their characteristics[J].International Journal Cast Metals Research,2008(1/4):156-161.
[8] GONG Wei-ping,CHEN Teng-fei,JIN Zhan-peng.Thermodynamic investigation of ZrO2-BaO system[J].中国有色金属学会会刊(英文版),2007(02):232-237.
[9] Erb A;Walker E;Flukiger R .The use of BaZrO3 crucibles in crystal growth of the high-Tc superconductors progress in crystal growth as well as in sample quality[J].Physica C:Superconductivity,1996,258(1/2):9-20.
[10] Srikanth Gopalan;Anil V. Virkar .Interdiffusion and Kirkendall effect in doped BaTiO{sub}3-BaZrO{sub}3 perovskites: effect of vacancy supersaturation[J].Journal of the American Ceramic Society,1999(10):2887-2899.
[11] Zhang Z;Xing F Y;Zhu M et al.Vacuum induction melting of TiNi alloys using BaZrO 3 crucibles[J].Materials Science Forum,2013,765:316-320.
[12] 戚宝德,缪卫东,王江波,冯昭伟,朱明.杂质对Ti-55.8%Ni SMA低周弯曲疲劳性能的影响[J].稀有金属,2008(02):252-256.
[13] Foroozmehr A;Kermanpur A;Ashrafizadeh F et al.Effects of thermo-mechanical parameters on microstructure and mechanical properties of Ti-50 at.%Ni shape memory alloy produced by VAR method[J].Materials Science and Engineering A,2012,535:164-169.
[14] Lin H C;Wu S K .The tensile behavior of a cold-rolled and reverse-transformed equiatomic TiNi alloy[J].ACTA METALLURGICA ET MATERIALIA,1994,42(5):1623-1630.
[15] 戚宝德 .杂质对Ti-55.8 wt%Ni SMA低周弯曲疲劳性能的影响[D].北京:北京有色金属研究总院,2006.
[16] 刘腾轼,杨弋涛.钼对含铌低合金铸钢碳化物析出行为的影响[J].铸造,2015(01):60-64.
[17] Brailovski V;Terriault P;Prokoshkin S .Influence of the post-deformation annealing heat treatment on the low-cycle fatigue of NiTi shape memory alloys[J].Journal of Materi-als Engineering and Performance,2002,11(6):614-621.
上一张 下一张
上一张 下一张
计量
  • 下载量()
  • 访问量()
文章评分
  • 您的评分:
  • 1
    0%
  • 2
    0%
  • 3
    0%
  • 4
    0%
  • 5
    0%