工程热物理学报 , 2003, 24(1): 82-84.
表面不透明三层漫反射散射性介质耦合换热
{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"以钙基蒙脱土为原料,采用微波-力化学法制备钠基蒙脱土(MMT).采用溶液离子交换法制备盐酸西替利嗪(CTH/MMT)纳米复合物,研究了MMT对CTH的吸附规律.利用XRD、FTIR、TG等分析了 CTH/MMT复合物的结构.通过体外人工模拟胃、肠液中的释放实验表征了CTH/MMT的缓释效果、缓释机制及其动力学.结果表明,CTH插层于MMT层间,层间距由1.25 nm增至2.13 nm.MMT对CTH插层吸附等温线符合Freundlich吸附等温方程,其吸附动力学符合二级动力学方程.体外的缓释试验表明,CTH/MMT具有良好的缓释效果,MMT可作为盐酸西替利嗪的控释载体材料.","authors":[{"authorName":"陈有梅","id":"277d4b2e-05e2-4cb8-8732-2f0d8ec4ddd7","originalAuthorName":"陈有梅"},{"authorName":"刘博","id":"438fed58-f5a6-43cd-abaf-bb09144ff049","originalAuthorName":"刘博"},{"authorName":"周安宁","id":"176bfd7a-83ed-4fd8-b5a3-6e68ad5b8ae8","originalAuthorName":"周安宁"},{"authorName":"梁俊","id":"9553fc53-03a2-4b72-8175-86f87aa4fcf6","originalAuthorName":"梁俊"}],"doi":"","fpage":"43","id":"4dd0ed87-8230-42a4-806e-beb6f3666cef","issue":"1","journal":{"abbrevTitle":"FHCLXB","coverImgSrc":"journal/img/cover/FHCLXB.jpg","id":"26","issnPpub":"1000-3851","publisherId":"FHCLXB","title":"复合材料学报"},"keywords":[{"id":"23ef28c6-eb92-4d17-a38e-da253a1ae0cd","keyword":"蒙脱土","originalKeyword":"蒙脱土"},{"id":"863cca5f-24d8-4798-b536-1cdfd83c084f","keyword":"盐酸西替利嗪","originalKeyword":"盐酸西替利嗪"},{"id":"4d60577d-262e-4e23-80f6-03624d5f586f","keyword":"微波","originalKeyword":"微波"},{"id":"333f7886-0d48-4b52-b80c-38b714ec748f","keyword":"吸附","originalKeyword":"吸附"},{"id":"11c70fdf-8757-48f6-b0eb-e8d44d58b742","keyword":"缓释","originalKeyword":"缓释"},{"id":"3606abdc-9454-47ca-be6f-07bf4b48f29b","keyword":"动力学","originalKeyword":"动力学"}],"language":"zh","publisherId":"fhclxb201001008","title":"盐酸西替利嗪/蒙脱土纳米复合物的制备及其结构与性能","volume":"27","year":"2010"},{"abstractinfo":"当前市场上的药品种类繁多,因此对不同厂商的同类药品进行识别分析对规范医药市场及保障人民用药安全有重要现实意义.实验采用基于傅里叶变换近红外漫反射光谱的光谱判别分析方法,结合矢量归一化方法和导数方法对光谱进行预处理,对不同品牌的盐酸左西替利嗪片建立定性识别模型,并用验证集样品对模型进行验证.验证结果表明,通过光谱库判别分析法建立识别模型不能正确识别同一厂家的两种样品,但对不同厂家盐酸左西替利嗪片的识别正确率为100％,该方法可以用于不同企业同类药品的快速定性识别和质量控制.","authors":[{"authorName":"陈芬芬","id":"705b1107-5dae-4531-bcf4-0141d7c3127d","originalAuthorName":"陈芬芬"},{"authorName":"高闽光","id":"1beaef1e-ebf7-4d41-afed-19e96bec1e01","originalAuthorName":"高闽光"},{"authorName":"徐亮","id":"1c41c0cf-20e8-4681-a753-62790ce1e5e0","originalAuthorName":"徐亮"}],"doi":"10.3969/j.issn.1007-5461.2015.01.001","fpage":"1","id":"4f0d7845-56e0-4621-bbe8-ea35e9d4dade","issue":"1","journal":{"abbrevTitle":"LZ","coverImgSrc":"journal/img/cover/LZ.jpg","id":"52","issnPpub":"1005-4006","publisherId":"LZ","title":"连铸"},"keywords":[{"id":"b58adcc7-9575-4ab6-b999-f1c29cc0f92e","keyword":"傅里叶光学","originalKeyword":"傅里叶光学"},{"id":"1793d2e0-459e-4115-82a7-7957a5f699aa","keyword":"近红外光谱","originalKeyword":"近红外光谱"},{"id":"522c8900-450d-495a-b13a-fa27f1b60434","keyword":"盐酸左西替利嗪片","originalKeyword":"盐酸左西替利嗪片"},{"id":"a23d1490-1301-463e-bae3-56b028df64ed","keyword":"判别分析","originalKeyword":"判别分析"},{"id":"0eb96020-460d-4dad-8ea0-094844afba0e","keyword":"快速鉴别","originalKeyword":"快速鉴别"}],"language":"zh","publisherId":"lzdzxb201501001","title":"基于近红外漫反射光谱的盐酸左西替利嗪片判别分析","volume":"32","year":"2015"},{"abstractinfo":"以三环类抗抑郁药盐酸阿米替林(Amitriptyline Hydrochloride,AH)为模型药物,海藻酸钠为内层,壳聚糖为外层,以乙二醇二缩水甘油醚(ethylene glycol diglycidyl ether,EGDE)为壳聚糖的交联剂,采用乳化分散-化学交联法,制备了盐酸阿米替林/海藻酸钠/壳聚糖微球,考察了其理化性质和释放性能. 结果表明,所得微球形状较规整,乳白色,平均粒径18.70 μm,载药量为9.5%,药物包封率达53.25%. XRD分析结果表明,微球内部盐酸阿米替林药物主要以无定形聚集态存在. 结果表明,盐酸阿米替林/海藻酸钠/壳聚糖微球有较好的药物缓释效果. 所制得的微球释药速率,随着海藻酸钠浓度增大而减慢;随反应pH值的增大而增大;随药物/海藻酸钠投料比的增大而增大. 在碱性和酸性缓冲溶液中,释药速率在酸性缓冲溶液中略大于碱性缓冲溶液中的释药速率.","authors":[{"authorName":"李国明","id":"ac25e3e1-a1d3-4fea-915b-5f73f2ce4545","originalAuthorName":"李国明"},{"authorName":"刘聪","id":"284d8561-a8fa-4f62-be52-6aa63a8f2b68","originalAuthorName":"刘聪"},{"authorName":"林跃","id":"11ea13a5-b24f-4c1f-999b-5a2ba8ffd55e","originalAuthorName":"林跃"},{"authorName":"高回春","id":"99bae4e1-0a01-4079-8082-b80f43c7418f","originalAuthorName":"高回春"},{"authorName":"骆小伟","id":"3fac8a0c-d06c-459c-aa9a-3b97f3bd5551","originalAuthorName":"骆小伟"},{"authorName":"汪朝阳","id":"afde2dbf-511b-459c-a6d0-057b7cf679e6","originalAuthorName":"汪朝阳"}],"doi":"10.3969/j.issn.1000-0518.2008.11.021","fpage":"1351","id":"e4285edd-72bb-41db-9bfa-267afabb07a4","issue":"11","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"26116298-f4a4-4176-91ae-a27015193bdf","keyword":"盐酸阿米替林","originalKeyword":"盐酸阿米替林"},{"id":"45ac8e77-19fb-47fc-ac08-6416097be57f","keyword":"海藻酸钠","originalKeyword":"海藻酸钠"},{"id":"ae16160e-b535-427a-9533-2f4c26fbe378","keyword":"壳聚糖","originalKeyword":"壳聚糖"},{"id":"ab2efe5f-3baa-421d-b916-ee028efb4392","keyword":"微球","originalKeyword":"微球"},{"id":"e5540b09-95b8-4750-ba61-effaaca7707d","keyword":"交联","originalKeyword":"交联"},{"id":"6d96ae66-2550-409a-9e67-0eeae86c6f60","keyword":"乙二醇二缩水甘油醚","originalKeyword":"乙二醇二缩水甘油醚"}],"language":"zh","publisherId":"yyhx200811021","title":"盐酸阿米替林/海藻酸钠/壳聚糖微球的制备及释放性能","volume":"25","year":"2008"},{"abstractinfo":"盐酸特拉唑嗪是一种新型选择性α1-肾上腺能受体拮抗剂，用于治疗高血压和良性前列腺增生。采用高效液相色谱-高分辨多级质谱（HPLC-HRMSn）联用法对强氧化条件下盐酸特拉唑嗪原料药的降解产物进行了详细的解析和结构确证。共检测到15种降解产物，其中7种与文献报道的有关物质相同，另外8种为新检测到的降解产物，其主要降解途径为酰胺键水解、羟基化、羰基化及3种途径组合的次级降解途径。","authors":[{"authorName":"孙玉明","id":"fb9d65ab-aaf9-4994-b82d-257c351a9add","originalAuthorName":"孙玉明"},{"authorName":"李英","id":"6975b971-0129-4e15-bbb4-2e8f81490c3a","originalAuthorName":"李英"},{"authorName":"王月月","id":"5bad92ff-aeef-4869-a791-00609f4d4ad8","originalAuthorName":"王月月"},{"authorName":"张华","id":"9b5947bc-fd65-4446-8b81-12e206fc871e","originalAuthorName":"张华"},{"authorName":"王玉林","id":"00c7f0c7-9fce-433f-b920-9f2f3973beaa","originalAuthorName":"王玉林"}],"doi":"10.3724/SP.J.1123.2015.12006","fpage":"490","id":"774f31a8-61a2-4d49-bd7b-a3d935c25074","issue":"5","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"038b13cb-64e2-415b-b626-375f6d91aadb","keyword":"高效液相色谱-高分辨多级质谱","originalKeyword":"高效液相色谱-高分辨多级质谱"},{"id":"170fedd3-0bc2-4966-b87f-30d39b4046bd","keyword":"结构鉴定","originalKeyword":"结构鉴定"},{"id":"b6c84520-d09c-4e3d-93f7-160a24695513","keyword":"降解产物","originalKeyword":"降解产物"},{"id":"4a8ae8e1-59c0-4e20-9ef5-cac1409553a8","keyword":"盐酸特拉唑嗪","originalKeyword":"盐酸特拉唑嗪"}],"language":"zh","publisherId":"sp201605007","title":"盐酸特拉唑嗪降解产物的结构鉴定","volume":"34","year":"2016"},{"abstractinfo":"研究了染料曙红B与盐酸异丙嗪的结合反应.在pH=3.50的Walpole介质中,曙红B本身的共振光散射信号较弱,与盐酸异丙嗪结合形成离子缔合物后,体系的共振光散射明显增强,并且光散射增强强度与盐酸异丙嗪在一定浓度范围内成正比,据此建立了一种高灵敏测定盐酸异丙嗪的方法.在体系的最大散射波长363 nm处,测得盐酸异丙嗪的线性范围为7.5×10-8～4.5×10-6 g/mL,检测限为1.8×10-8 g/mL,用于盐酸异丙嗪片剂、针剂、人血清及尿样中盐酸异丙嗪的测定,结果令人满意.","authors":[{"authorName":"冯素玲","id":"97451c88-03c0-4f6a-bf3f-949237513e7f","originalAuthorName":"冯素玲"},{"authorName":"PAN Zi-Hong","id":"0f77f091-434f-49e7-9edc-6065cd3d8934","originalAuthorName":"PAN Zi-Hong"},{"authorName":"潘自红","id":"cfce1571-2b1b-4c4e-8069-f6ec702dd95d","originalAuthorName":"潘自红"},{"authorName":"樊静","id":"e52b7a00-c9ac-456b-9fc5-521c8abfc4c2","originalAuthorName":"樊静"}],"doi":"10.3969/j.issn.1000-0518.2008.12.015","fpage":"1444","id":"b06218e1-27a2-422a-a6a1-e1c0b15b46f1","issue":"12","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"55d0636b-4d44-4dab-abdf-3030a8612fb5","keyword":"盐酸异丙嗪","originalKeyword":"盐酸异丙嗪"},{"id":"121908fc-0ab4-4aac-8f62-a31cfd00d354","keyword":"曙红B","originalKeyword":"曙红B"},{"id":"94da5d7e-558c-41db-aa50-5c1962430d83","keyword":"共振光散射","originalKeyword":"共振光散射"}],"language":"zh","publisherId":"yyhx200812015","title":"曙红B共振光散射法测定微量的盐酸异丙嗪","volume":"25","year":"2008"},{"abstractinfo":"在酸性条件下,盐酸二氧丙嗪分子中氮原子被质子化后与阴离子AuCl-4形成离子缔合物,缔合物又被二氯甲烷带入鲁米诺的氯化十六烷基三甲基铵反胶束纳米微反应器中,离解出的AuCl-4立即与鲁米诺产生化学发光.在一定浓度范围内,发光强度与盐酸二氧丙嗪的含量呈线性关系,可间接测定盐酸二氧丙嗪的含量.在HCI、AuCl-4、鲁米诺、碳酸钠分别为0.05 mol/L、20 mg/L、0.4×10-4mol/L和0/3 mol/L(pH=11.5),R([H2O]/[CTAC])值为11,泵速均为3.6 mL/min(单管),聚四氟乙烯管的内径为0.8 mm,进样体积为120 μL,e至流通池间的距离为8 cm,反应盘管的长度为120 mm,直径为2 mm,负高压为-650 V,二氯甲烷为萃取剂的条件下.线性范围为0.001-20 mg/L,检出限(3σ)为0.06μg/L,对质量浓度为1.0 mg/L的盐酸二氧丙嗪进行11次平行测定,RSD为1.4％.方法可用于片剂和生物体液中盐酸二氧丙嗪的测定.","authors":[{"authorName":"石文兵","id":"d4f73250-7a09-4c75-b56c-f8c41abd77f0","originalAuthorName":"石文兵"}],"doi":"10.3969/j.issn.1000-0518.2008.04.014","fpage":"441","id":"3c8a9875-9832-45f2-8689-e7f169a378c8","issue":"4","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"80762fd7-abb8-4465-87c7-ba452c75b955","keyword":"纳米微反应器","originalKeyword":"纳米微反应器"},{"id":"54eefd0c-c745-4436-9574-13db65c8b9c9","keyword":"盐酸二氧丙嗪","originalKeyword":"盐酸二氧丙嗪"},{"id":"741361ea-183c-44bb-9ca2-467033f93b34","keyword":"化学发光","originalKeyword":"化学发光"}],"language":"zh","publisherId":"yyhx200804014","title":"流动注射纳米微反应器化学发光法测定盐酸二氧丙嗪","volume":"25","year":"2008"},{"abstractinfo":"建立了高效液相色谱柱前衍生化法测定大鼠腹腔注射(i.p.)给药盐酸氟西汀前后脑渗析液中5-羟色胺(5-HT)的浓度变化情况.在大鼠给药盐酸氟西汀前和给药后不同时间点取其脑渗析液,加入衍生化试剂反应后,以乙腈-20 mmol/L醋酸盐缓冲液(pH 5.0)(体积比为45:55)(含20 mmol/L辛烷磺酸钠)作为流动相,在HypersilC18色谱柱(250 mm×2.0 mm,5μm)上进行分离,荧光检测波长为λex=330 nm,λem=455 nm.5-HT在浓度为0.25～5.0 nmol/L范围内线性关系良好(r=0.999 1);5-HT的最低定量限为0.25 nmol/L.本法准确可靠、简便,适用于生物样品中5-HT的浓度测定.","authors":[{"authorName":"郭云珍","id":"f7155e3d-abd6-4478-9ee2-a17b08a9f8f9","originalAuthorName":"郭云珍"},{"authorName":"于莉","id":"63ca6b01-93ad-4068-9df1-0f464e2398cb","originalAuthorName":"于莉"},{"authorName":"马郑","id":"6ec14a2c-0a0d-4692-8e3d-2a6afa4ccc34","originalAuthorName":"马郑"},{"authorName":"郭兴杰","id":"2430771c-ce12-4448-bb54-dc8c3eb398de","originalAuthorName":"郭兴杰"}],"doi":"10.3321/j.issn:1000-8713.2007.02.017","fpage":"211","id":"47d56f7f-1d57-4a1e-bb79-a7b40b6ab485","issue":"2","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"fbafb7f3-95e1-489a-b8f9-f0fa2bfe7990","keyword":"柱前衍生化","originalKeyword":"柱前衍生化"},{"id":"a6a27e5c-324f-430a-a62c-ec7ca317c7ed","keyword":"高效液相色谱","originalKeyword":"高效液相色谱"},{"id":"4f7559e4-9e70-48f8-8b87-85c9f0d59caf","keyword":"荧光检测","originalKeyword":"荧光检测"},{"id":"feecf34c-211d-471f-80c1-49f5e30b7fc5","keyword":"5-羟色胺","originalKeyword":"5-羟色胺"},{"id":"fa001da8-d2ea-4fb1-9eb8-41787fb1885c","keyword":"盐酸氟西汀","originalKeyword":"盐酸氟西汀"}],"language":"zh","publisherId":"sp200702017","title":"高效液相色谱法测定大鼠给药盐酸氟西汀后脑渗析液中的5-羟色胺","volume":"25","year":"2007"},{"abstractinfo":"以自制的限进性填料柱为预处理富集柱,Luna C18柱为分析柱,通过柱切换技术将限进性填料柱与高效液相色谱联用(RAM-HPLC),研究了盐酸贝那普利的在线富集效果.考察了进样体积与峰面积、系统总压力的关系,以及常规进样与大体积进样的差别.当进样体积在100 μL以内时,峰面积随进样体积的增加而增加；当进样体积大于80 μL时,系统总压力变化明显.考虑对整个系统的保护,选择80μL作为最大进样体积.同一浓度的样品进样20μL与进样80 μL所得峰面积之间的线性关系良好.RAM柱对盐酸贝那普利具有良好的富集作用,能够有效提高HPLC的灵敏度,而且具有简单、经济的特点.","authors":[{"authorName":"张晓惠","id":"7ab33d37-696f-45e2-8a66-11a884439594","originalAuthorName":"张晓惠"},{"authorName":"王荣","id":"af6eed52-a6a3-4717-a0af-412236f5185c","originalAuthorName":"王荣"},{"authorName":"谢华","id":"f479b34b-19ee-491c-ad54-0ec52e74ccaf","originalAuthorName":"谢华"},{"authorName":"尹强","id":"a2c40962-5220-46e0-9151-06dc6c8d37f6","originalAuthorName":"尹强"},{"authorName":"李晓云","id":"37d5dc95-9bfa-45ca-b2d3-8262be16bc37","originalAuthorName":"李晓云"},{"authorName":"贾正平","id":"40cbc708-4a37-47df-b893-6cc2926c3778","originalAuthorName":"贾正平"},{"authorName":"武晓玉","id":"8eae59bc-3b1a-47c0-a723-658a9ce2b165","originalAuthorName":"武晓玉"},{"authorName":"张娟红","id":"e5124d9b-9223-4948-a32b-d19c362c13f0","originalAuthorName":"张娟红"},{"authorName":"李文斌","id":"4ce41af9-b3e6-432e-929f-ef62e4e1f449","originalAuthorName":"李文斌"}],"doi":"10.3724/SP.J.1123.2012.11021","fpage":"451","id":"33f92ef9-f93e-492f-a9fd-b773b4807b52","issue":"5","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 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