采用自制的硬质阳极氧化装置,在铝合金6061薄板表面沿着铝基体方向形成较大的温度梯度降温条件,对铝板进行硫酸硬质氧化试验。对氧化膜形貌、硬度、膜厚分别进行了观察和分析。结果表明,相同条件下,采用温度梯度法制备的硬质阳极氧化膜,其均匀性、膜的厚度和硬度都大大优于传统的硬质阳极氧化膜,膜的质量得到很大的提高。
The hard anodic oxidation film on 6061 aluminum alloy sheet surface was prepared by a self-made hard anodic oxidation device under the conditions of large temperature gradient along the direction of aluminum matrix.The oxide film morphology,hardness and thickness were observed and analyzed.The results showed that after hard anodizing the aluminium sheet the film quality was greatly improved,the thickness,hardness and uniformity of hard anodic oxide film prepared with temperature gradient method were far superior to that of the traditional hard anodic oxide film.
参考文献
[1] | Grzegorz D. Sulka;Wojciech J. Stepniowski .Structural features of self-organized nanopore arrays formed by anodization of aluminum in oxalic acid at relatively high temperatures[J].Electrochimica Acta,2009(14):3683-3691. |
[2] | Zaraska, L;Sulka, GD;Jaskula, M .The effect of n-alcohols on porous anodic alumina formed by self-organized two-step anodizing of aluminum in phosphoric acid[J].Surface & Coatings Technology,2010(11):1729-1737. |
[3] | Jian-hua Liu,Ming Li,Song-mei Li,Min Huang.Effect of the microstructure of Al 7050-T7451 on anodic oxide formation in sulfuric acid[J].矿物冶金与材料学报,2009(04):432-438. |
[4] | 孙衍乐,宣天鹏,徐少楠,张敏.铝合金的阳极氧化及其研发进展[J].电镀与精饰,2010(04):18-21. |
[5] | 高丽,黎学明,李武林,杨文静.LY12铝合金低温硬质阳极氧化工艺研究[J].表面技术,2010(06):90-92,96. |
[6] | 王平,魏晓伟,安家菊.汽车空调涡旋盘快速硬质阳极氧化处理工艺研究[J].汽车技术,2006(08):30-33. |
[7] | 查康,顾琳.不同硫酸浓度对2A12脉冲硬质阳极氧化工艺的影响[J].铸造技术,2008(07):952-954. |
[8] | 董春晓,李淑英,谢品品,范洪强.有机添加剂对铝阳极氧化膜性能的影响[J].腐蚀与防护,2010(03):216-219. |
[9] | Mark Jozefowicz .Coat Aluminum Anodizing: The low-down on how anodizers can get their feet wet and enter the lucrative hard coat market[J].Metal finishing,2005(10):39-40. |
[10] | 张永光,张燎原.宽温快速铝合金阳极氧化添加剂[J].安徽工业大学学报(自然科学版),2002(02):112-114. |
[11] | 左焕然,魏晓伟.2A12低H2SO4浓度的硬质阳极氧化膜结构研究[J].表面技术,2008(03):30-32. |
[12] | 刘晓旭 .LY12铝合金不同硫酸浓度的阳极氧化膜结构研究[D].西华大学,2007. |
[13] | 王剑,魏晓伟.H2SO4浓度对6061硬质阳极氧化膜层质量的影响[J].西华大学学报(自然科学版),2009(02):100-102. |
[14] | 王平,魏晓伟.活塞阳极氧化表面气泡形成的机理及影响[J].材料保护,2005(10):54-57. |
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