采用磁控溅射法在不锈钢表面制备了TiAlN涂层,采用压入法及划痕法表征了涂层的结合强度.分析表明,压入法只能作为一种定性的测定方法,该法测得TiAlN涂层的结合强度达到HF3.划痕法结合了声信号、摩擦力信号和划痕微观形貌,可以定量测定结合强度,该法测得在压头曲率半径为200μm的情况下,TiAlN涂层的临界载荷达到13 N,比传统TiN涂层提高了45％.
参考文献
| [1] | Zhou Z.;Rainforth WM.;Lewis DB.;Creasy S.;Forsyth JJ.;Clegg E. Ehiasarian AR.;Hovespian PE.;Munz WD. .Oxidation behaviour of nanoscale TiAlN/VN multilayer coatings[J].Surface & Coatings Technology,2004(0):198-203. |
| [2] | HARRIS S G;DOYLE E D;VLASVELD A C et al.A Study of the Wear Mechanisms of Ti1-x AlxN and Ti1-x-y AlxCryN Coated High-speed Steel Twist Drills under Dry Machining Conditions[J].WEAR,2003,254(07):723-734. |
| [3] | HALKER P R;BULL S J;RICKERBY D S .A Review of the Methods for the Evaluation of Coating-substrate Adhesion[J].MATERIALS SCIENCE & ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING,1991,140:583-592. |
| [4] | JACOBSON R .Measurement of the Adhesion of Thin Films[J].THIN SOLID FILMS,1976,34(02):191-199. |
| [5] | VALLI J .A Review of Adhesion Test Methods for Thin Hard Coatings[J].Vacuum Surfaces and Films,1986,4(06):3007-3014. |
| [6] | 朱晓东,米彦郁,胡奈赛,何家文.膜基结合强度评定方法的探讨-划痕法、压入法、接触疲劳法测定的比较[J].中国表面工程,2002(04):28-31. |
| [7] | 马峰,蔡珣.膜基界面结合强度表征和评价[J].表面技术,2001(05):15-19. |
| [8] | 倪晟,孙卓,赵强.磁控共溅射制备氮化钛铝薄膜及其机械性能的研究[J].功能材料,2005(12):1842-1844,1848. |
| [9] | PalDey S.;Deevi SC. .Single layer and multilayer wear resistant coatings of (Ti,Al)N: a review [Review][J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,2003(1/2):58-79. |
| [10] | Xie Y.;Hawthorne HM. .A model for compressive coating stresses in the scratch adhesion test[J].Surface & Coatings Technology,2001(1):15-25. |
| [11] | 江范清 .划痕法评价氮化钛结合力的研究[D].成都:西南交通大学,2012. |
| [12] | J. Stallard;S. Poulat;D. G. Teer .The study of the adhesion of a TiN coating on steel and titanium alloy substrates using a multi-mode scratch tester[J].Tribology International,2006(2):159-166. |
| [13] | 李明升,陈柯伟,王福会,徐家寅.空心阴极离子镀TiAlN复合薄膜结构及抗氧化性能的研究[J].腐蚀科学与防护技术,2001(z1):411-414,486. |
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