{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"在pH值为1.0的HCl-KCl、pH值为8.0的HCl-三羟甲基氨基甲烷(tris)缓冲溶液和Tween80胶束介质中,分别研究了1-亚硝基-2-萘酚(NN)与Fe(Ⅲ)、Ni(Ⅱ)的显色反应.建立了胶束紫外-可见分光光度法测定微量Fe(Ⅲ)、Ni(Ⅱ)的新方法.结果表明,Fe(Ⅲ)-NN(pH值为1.0)、Ni(Ⅱ)-NN(pH值为8.0)配合物的最大吸收波长分别为445 nm和455 nm;摩尔吸光系数分别为1.68×104 L/(mol·cm)和1.01×104 L/(mol·cm);检出限分别为0.025 mg/L和0.040 mg/L;有色溶液的吸光度与Fe(Ⅲ)量在0.5~2.5 mg/L、与Ni(Ⅱ) 量在0.2~1.0 mg/L范围内符合比耳定律,加标回收率为97.8%~103.5 %(n=6).本法较好地测定了非晶态FeNiCr合金钢中的铁和镍.","authors":[{"authorName":"夏畅斌","id":"85e19d77-fbb0-402d-a316-755c320fbd6b","originalAuthorName":"夏畅斌"},{"authorName":"何湘柱","id":"707cf177-5d18-4297-b62a-6ffaa5990817","originalAuthorName":"何湘柱"},{"authorName":"李浔","id":"d1b78b32-b33d-40ab-b8d0-f6c77454c32b","originalAuthorName":"李浔"}],"doi":"10.3969/j.issn.1001-1560.2006.03.022","fpage":"72","id":"81db63a5-8452-4922-a805-2c44af1ad1ab","issue":"3","journal":{"abbrevTitle":"CLBH","coverImgSrc":"journal/img/cover/CLBH.jpg","id":"7","issnPpub":"1001-1560","publisherId":"CLBH","title":"材料保护"},"keywords":[{"id":"e9d45213-4975-4c94-bbe0-6088f1b1a250","keyword":"元素测定","originalKeyword":"元素测定"},{"id":"e85763ba-a2b6-4ba5-ad6f-e9608a78d4ff","keyword":"铁","originalKeyword":"铁"},{"id":"34b8c00b-e900-4314-a7ef-09fb250e2f11","keyword":"镍","originalKeyword":"镍"},{"id":"acf51cd7-2fc6-43d6-b4da-84c3085d9266","keyword":"紫外-可见分光光度法","originalKeyword":"紫外-可见分光光度法"},{"id":"d13f6f8d-1235-4b5b-b2c8-849a11724b95","keyword":"非晶态合金钢","originalKeyword":"非晶态合金钢"},{"id":"f2f774c4-57e7-4dcf-a46e-62f2db7c34fb","keyword":"1-亚硝基-2-萘酚","originalKeyword":"1-亚硝基-2-萘酚"}],"language":"zh","publisherId":"clbh200603022","title":"用胶束光度法测定非晶态FeNiCr合金中的铁和镍","volume":"39","year":"2006"},{"abstractinfo":"采用原位分析技术对不同结晶态的低合金钢连铸方坯的成分分布、偏析、疏松、夹杂和其他缺陷进行了分析.分析结果证明,具有较高的等轴晶率的方坯具有较均匀的成分分布和较少的缺陷.","authors":[{"authorName":"杨志军","id":"f6c12e8e-f707-4f89-9845-8aaf65488922","originalAuthorName":"杨志军"},{"authorName":"王海舟","id":"63e1e689-755d-4828-a0bf-2a37935b33ca","originalAuthorName":"王海舟"}],"doi":"","fpage":"67","id":"b50d8f03-111d-4d12-b8db-93269bf0b371","issue":"9","journal":{"abbrevTitle":"GT","coverImgSrc":"journal/img/cover/GT.jpg","id":"27","issnPpub":"0449-749X","publisherId":"GT","title":"钢铁"},"keywords":[{"id":"ddba5084-2da0-4ae1-9f75-74f0965eb616","keyword":"原位分析","originalKeyword":"原位分析"},{"id":"d819245d-5e50-48ce-99be-cd946e27fc8f","keyword":"夹杂物","originalKeyword":"夹杂物"},{"id":"6a2f614f-71e6-46fa-8571-ccfd843ffb10","keyword":"方坯","originalKeyword":"方坯"}],"language":"zh","publisherId":"gt200309016","title":"不同结晶态合金钢方坯的原位分析","volume":"38","year":"2003"},{"abstractinfo":"介绍一种制备大块非晶态合金的新方法一快淬非晶态合金条带高压复合法其原理是利用高压抑制非晶态合金的晶化过程,从而在较宽的温区通过大量均匀的粘滞流变实现快淬非晶态合金条带的全致密复合非晶态Ni_69Cr_7Fe_2.5Si_8B_13.5合金在压力为1.5GPa时,其粘滞流变温区增至约60K,在压结温度为733~773K内可获得完全密实(理论密度的99%以上)的块状非晶态样品","authors":[{"authorName":"周飞","id":"6ded4fd9-d2ad-4498-b894-69ba7730d9d9","originalAuthorName":"周飞"},{"authorName":"卢柯","id":"7f4e4720-ca14-4901-b1e3-4b350e1b8c82","originalAuthorName":"卢柯"}],"categoryName":"|","doi":"","fpage":"127","id":"9c153da8-ecd0-4810-9371-0a53a4b3ab21","issue":"2","journal":{"abbrevTitle":"CLYJXB","coverImgSrc":"journal/img/cover/CLYJXB.jpg","id":"16","issnPpub":"1005-3093","publisherId":"CLYJXB","title":"材料研究学报"},"keywords":[{"id":"db096057-f2ca-40da-85b7-342ee0c38330","keyword":"块状非晶态合金","originalKeyword":"块状非晶态合金"},{"id":"c0df90e8-31fc-403d-b166-c80f44fc0ba0","keyword":"null","originalKeyword":"null"},{"id":"01ce1140-5390-44e6-967c-b45230568b91","keyword":"null","originalKeyword":"null"}],"language":"zh","publisherId":"1005-3093_1997_2_10","title":"非晶态合金条带高压复合法制备大块非晶态合金","volume":"11","year":"1997"},{"abstractinfo":"本文提出在非晶态合金的形成中,元素的原子半径采用实测的原子间距之半来衡量。在总结归纳大量实验资料的基础上发现二元或多元非晶态合金,其组成元素的尺寸因素(ΔR/R_i)都大于9%(个别例外)。分析了影响形成二元非晶态合金的因素,得到了形成二元非晶态合金的必要条件为:","authors":[{"authorName":"张邦维","id":"d6ec70c8-d82e-4baa-aea5-44084f848484","originalAuthorName":"张邦维"}],"categoryName":"|","doi":"","fpage":"285","id":"4a8047f8-a949-4543-8927-8b88a4123914","issue":"3","journal":{"abbrevTitle":"JSXB","coverImgSrc":"journal/img/cover/JSXB.jpg","id":"48","issnPpub":"0412-1961","publisherId":"JSXB","title":"金属学报"},"keywords":[{"id":"4037bca1-3c57-4a8c-89ce-35acee82fff6"}],"language":"zh","publisherId":"0412-1961_1981_3_6","title":"尺寸因素在非晶态合金形成中的作用","volume":"17","year":"1981"},{"abstractinfo":"非晶态合金已在金属应用领域占据了重要的地位.为了对非晶态合金镀层屏蔽材料进行优化设计,首先对典型非晶态合金镀层屏蔽效能进行实验测量和优化分析,确定了影响镀层屏蔽效能的各主要因素,最终得出了满足要求的最佳施镀工艺,为非晶态合金在电磁屏蔽领域的广泛应用奠定了理论基础.同时,为非晶态合金镀层更好地应用于其它领域提供了一种可行的通用性优化方法.","authors":[{"authorName":"甄建伟","id":"d1357390-69f2-49cb-804e-b03153e09acd","originalAuthorName":"甄建伟"},{"authorName":"安振涛","id":"42ad10aa-932b-45e1-a963-d52b5d6b885b","originalAuthorName":"安振涛"},{"authorName":"张勇","id":"be9d874d-7926-4162-ab3f-7a6baf34f948","originalAuthorName":"张勇"},{"authorName":"闫军","id":"bfb3ac03-62b3-4149-91c2-85ec96011c6a","originalAuthorName":"闫军"}],"doi":"","fpage":"428","id":"3a363f65-aa6d-433d-b6bd-ff1e8c050251","issue":"z3","journal":{"abbrevTitle":"GNCL","coverImgSrc":"journal/img/cover/GNCL.jpg","id":"33","issnPpub":"1001-9731","publisherId":"GNCL","title":"功能材料"},"keywords":[{"id":"48eef8ae-2e95-4725-aa41-003c0766af5d","keyword":"非晶态合金","originalKeyword":"非晶态合金"},{"id":"14c441ca-8f32-4473-90bb-97f0ae133a26","keyword":"屏蔽材料","originalKeyword":"屏蔽材料"},{"id":"4602c8bc-ba8c-4e06-8500-6e77ab056171","keyword":"弹药包装","originalKeyword":"弹药包装"},{"id":"19a78059-2829-433b-ab61-f47d23e0bfbd","keyword":"优化","originalKeyword":"优化"}],"language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communication, consumer electronics products)领域有重大发展潜力.","authors":[{"authorName":"王晓军","id":"119cb991-d439-4e65-aaa7-05d2a5ff76e3","originalAuthorName":"王晓军"},{"authorName":"陈学定","id":"840aa18c-d1d6-4e5c-846e-2ab344ea774c","originalAuthorName":"陈学定"},{"authorName":"王晓丽","id":"b9ee5dc4-3d27-4b8b-9d64-6fc6bad23e11","originalAuthorName":"王晓丽"},{"authorName":"夏天东","id":"e01b800c-aa50-4cbd-86e1-5b7b09c1e5fc","originalAuthorName":"夏天东"},{"authorName":"俞伟元","id":"422fcd38-85ef-42bd-9509-30320a5e841e","originalAuthorName":"俞伟元"}],"doi":"","fpage":"77","id":"dd167de1-9ed1-40a2-9822-079cc4588edf","issue":"4","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"34f3e363-92fe-4a04-9276-5ec2df9008ec","keyword":"大块非晶","originalKeyword":"大块非晶"},{"id":"47fe6992-b188-4e44-80d9-17edc1166da3","keyword":"镁基非晶态合金","originalKeyword":"镁基非晶态合金"},{"id":"758c9761-e3b8-4155-aa34-325ab02e3ac0","keyword":"镁合金","originalKeyword":"镁合金"}],"language":"zh","publisherId":"cldb200404023","title":"大块镁基非晶态合金的研究进展","volume":"18","year":"2004"},{"abstractinfo":"介绍了非晶态合金催化剂的制备方法,其中,化学沉积负载法和添加第三组分化学沉积法制得的催化剂具有优良的催化活性和抗毒化能力,以及很高的热稳定性,因此这两种方法近年来备受关注.简述了非晶态合金催化剂在CO、CO2、烯烃、炔烃、苯、含氧或含氮化合物等的加氢反应以及析氢电催化反应中的应用;分析了现阶段非晶态合金催化剂制备和应用存在的问题,并展望了其前景.","authors":[{"authorName":"姬文晋","id":"e28954c7-1199-4ae1-afdd-f6e0e5bf25a3","originalAuthorName":"姬文晋"},{"authorName":"黄慧民","id":"e35c70b9-981d-492b-88a4-a938ff1207a7","originalAuthorName":"黄慧民"},{"authorName":"邓淑华","id":"882d8d3e-cd41-4d8c-903c-bcd1ab66524e","originalAuthorName":"邓淑华"},{"authorName":"郑育英","id":"35568f67-9e0e-4d47-ab71-5efdeab57d92","originalAuthorName":"郑育英"},{"authorName":"欧得华","id":"db06c1d1-59a2-4b9e-ac6f-d1bdeb81cd79","originalAuthorName":"欧得华"}],"doi":"","fpage":"73","id":"34c82124-8adb-43f2-b6c0-dc96f348a84d","issue":"5","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"e13a2f77-b6c1-4810-9a94-95d4e34c1919","keyword":"非晶态合金","originalKeyword":"非晶态合金"},{"id":"ea394069-6de5-40e2-af60-b00755e4a78e","keyword":"催化剂","originalKeyword":"催化剂"},{"id":"987eb6bf-e194-4550-809c-afdc19730a6d","keyword":"制备方法","originalKeyword":"制备方法"},{"id":"2c44c5eb-9905-4648-ad26-b3e78db3ebd1","keyword":"加氢","originalKeyword":"加氢"},{"id":"bea05150-40d5-45b1-bcd1-402fdcaafdaa","keyword":"析氢","originalKeyword":"析氢"}],"language":"zh","publisherId":"cldb200605021","title":"非晶态合金催化剂制备及其应用","volume":"20","year":"2006"}],"totalpage":4006,"totalrecord":40057}