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以Ti和B4C为起始反应物,分别在常规和超重力条件下通过燃烧合成技术制备出Ti(C,N)-TiB2复合粉体,利用XRD和SEM对燃烧产物进行了表征,研究了起始组成和超重力条件对燃烧产物相组成和微观形貌的影响.结果表明,燃烧产物主要由Ti(C,N)和TiB2组成,通过改变起始配方中Ti/B4C的摩尔比,可以调节产物中Ti(C,N)和TiB2的相对含量.超重力条件下,反应物颗粒接触更加充分,碰撞更加频繁,因而晶粒形态发育更加完整,生成规则的多面体.

参考文献

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