{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"以乙酸乙酯为溶剂,马来酸酐、乙醇胺、苯乙烯为单体,过氧化苯甲酰为引发剂,采用溶液聚合法合成了聚羧酸型马来酸酐-乙醇胺-苯乙烯(MA-EA-St)高分子分散剂,研究了聚合反应温度和时间、引发剂用量及酰化马来酸酐与苯乙烯的摩尔比对TiO2颗粒悬浮率的影响,获得了较佳的聚合反应条件为∶n(酰化马来酸酐)∶n(苯乙烯)=1.25,聚合反应温度75℃、时间5h,引发剂用量占单体总质量的2%.当此条件下合成的MA-EA-St分散剂用量为2.5 g/L时,TiO2颗粒的悬浮率为97.42%,达到较佳的分散效果.","authors":[{"authorName":"刁丽","id":"0816ef43-c8c4-4891-a4d4-3e1859abfba7","originalAuthorName":"刁丽"},{"authorName":"曹亚峰","id":"9def552f-b2cd-4f03-ab8a-afbf8a978576","originalAuthorName":"曹亚峰"}],"doi":"","fpage":"61","id":"e3fdf271-73d2-471d-9f97-e3731c021aad","issue":"3","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰 "},"keywords":[{"id":"16188dbb-2949-402b-adee-2a8512b2080b","keyword":"颜料","originalKeyword":"颜料"},{"id":"b31ba932-bfff-4fcd-955e-87c899d39ad7","keyword":"二氧化钛","originalKeyword":"二氧化钛"},{"id":"809ac25f-0d06-4efd-bc79-026a7b142eb6","keyword":"分散剂","originalKeyword":"分散剂"},{"id":"af08f7ec-b91b-49e6-9773-a1bfe978cd04","keyword":"马来酸酐","originalKeyword":"马来酸酐"},{"id":"954a4239-45b8-4c99-b43d-c236d044196e","keyword":"乙醇胺","originalKeyword":"乙醇胺"},{"id":"0573eb6b-d71d-4bcf-baa2-4beac8b5c209","keyword":"酰化","originalKeyword":"酰化"},{"id":"ddbef852-36d6-45d8-a28b-cc27797a1fab","keyword":"苯乙烯","originalKeyword":"苯乙烯"},{"id":"93f3bfb0-69b0-4ae4-9586-9c4f8f6a4862","keyword":"聚合","originalKeyword":"聚合"}],"language":"zh","publisherId":"ddyts201203016","title":"颜料分散用马来酸酐-乙醇胺-苯乙烯水性高分子助剂的合成","volume":"31","year":"2012"},{"abstractinfo":"采用熔融接枝法在Haake转距流变仪上进行SEBS接枝马来酸酐(MAH)的反应,通过FT-IR验证了SEBS接枝产物的产生.用酸碱滴定法和FT-IR测定SEBS-g-MAH的接枝率,同时考察不同反应条件:反应时间、反应温度、MAH量、过氧化二异丙苯(DCP)量对SEBS-g-MAH的接枝率和接枝效率的影响.实验结果证明,SEBS接枝MAH的优化反应条件是:反应时间为10 min,反应温度为160 ℃,MAH量为6%,DCP量为 0.55%.","authors":[{"authorName":"郭艳","id":"b32ea110-6efb-4fe7-a580-b2c8ffbc6acc","originalAuthorName":"郭艳"},{"authorName":"蒋遥明","id":"a6dbfe24-5136-489b-81f2-28ac0e079bad","originalAuthorName":"蒋遥明"},{"authorName":"张爱民","id":"d86c87c2-b353-4fd1-9c88-84ee07395e5a","originalAuthorName":"张爱民"}],"doi":"","fpage":"88","id":"91359626-9633-4403-ab89-f0f585e40b34","issue":"6","journal":{"abbrevTitle":"GFZCLKXYGC","coverImgSrc":"journal/img/cover/GFZCLKXYGC.jpg","id":"31","issnPpub":"1000-7555","publisherId":"GFZCLKXYGC","title":"高分子材料科学与工程"},"keywords":[{"id":"58326b92-19b3-46f9-9ff1-ccd61986dfc9","keyword":"SEBS","originalKeyword":"SEBS"},{"id":"38c745f2-092f-429f-94b6-1678048b24f9","keyword":"熔融接枝","originalKeyword":"熔融接枝"},{"id":"79c9283b-1727-4d23-9b89-934f1718e4e0","keyword":"马来酸酐","originalKeyword":"马来酸酐"},{"id":"e3a492de-28bc-4b66-a9ec-06c08fbf5874","keyword":"FT-IR","originalKeyword":"FT-IR"},{"id":"fd694446-aa60-49ed-b05c-699bff8b4fce","keyword":"酸碱滴定","originalKeyword":"酸碱滴定"}],"language":"zh","publisherId":"gfzclkxygc200306022","title":"SEBS熔融接枝马来酸酐的研究","volume":"19","year":"2003"},{"abstractinfo":"采用玉米淀粉为原料,马来酸酐(MAH)为酯化剂,通过干法制备马来酸酐酯化淀粉,研究了MAH用量对酯化淀粉性能的影响.利用红外光谱法(FT-IR)对原淀粉和酯化淀粉进行扫描,结果证明MAH成功与淀粉发生酯化反应并接枝到淀粉结构上.并利用化学滴定法、激光粒度仪、X射线衍射法(XRD)、差示扫描量热法(DSC)和热重分析(TGA)对不同MAH用量制得的酯化淀粉进行了分析.结果表明,干法酯化淀粉的取代度随MAH用量的增多逐渐增大,MAH用量超过m(MAH)/m(淀粉)=20/100后,取代度趋于稳定.酯化淀粉的性能与其取代度密切相关,酯化淀粉的分子链随取代度增大而增长,从而使粒径及其分布率增大,结晶度降低,糊化温度降低,以及热稳定性变差.","authors":[{"authorName":"左迎峰","id":"69c3371d-5d03-47eb-97a8-33458ebbac89","originalAuthorName":"左迎峰"},{"authorName":"顾继友","id":"67bd3e6c-b527-4165-b020-d414cd8304ee","originalAuthorName":"顾继友"},{"authorName":"杨龙","id":"25fe3a0b-a6cf-49fa-a739-b853774b9833","originalAuthorName":"杨龙"},{"authorName":"谭海彦","id":"fb87426a-05ff-41f0-9c2a-bfe90b58b14d","originalAuthorName":"谭海彦"},{"authorName":"张彦华","id":"997f8149-ad06-42ac-bef0-5fbb2252f946","originalAuthorName":"张彦华"}],"doi":"","fpage":"162","id":"5fea9499-10a7-432b-af48-3bd227e38133","issue":"1","journal":{"abbrevTitle":"GFZCLKXYGC","coverImgSrc":"journal/img/cover/GFZCLKXYGC.jpg","id":"31","issnPpub":"1000-7555","publisherId":"GFZCLKXYGC","title":"高分子材料科学与工程"},"keywords":[{"id":"f93163f4-c97b-4729-84f4-82719a2cb008","keyword":"玉米淀粉","originalKeyword":"玉米淀粉"},{"id":"15b45a52-11fc-4b9b-bbf6-5f603093f610","keyword":"马来酸酐","originalKeyword":"马来酸酐"},{"id":"d27f2f9b-9d94-448d-9c71-a85f5574a2d6","keyword":"用量","originalKeyword":"用量"},{"id":"09b60ad7-00ee-4fe6-8053-b3c6d5e80ed3","keyword":"干法酯化","originalKeyword":"干法酯化"},{"id":"a8310c1b-bfbb-42e6-8fae-b9f053d10eeb","keyword":"性能","originalKeyword":"性能"}],"language":"zh","publisherId":"gfzclkxygc201401036","title":"马来酸酐用量对干法制备马来酸酐淀粉酯性能的影响","volume":"30","year":"2014"},{"abstractinfo":"研究了微悬浮体系下辐射引发乙丙橡胶接枝马来酸酐.以二甲苯为溶剂制备了乙丙橡胶和马来酸酐的微悬浮体系,采用动态光散射测得该体系下的粒径分布为5~7μm.考察了辐射剂量和单体浓度对马来酸酐接枝率的影响.结果表明,微悬浮下共辐射能明显提高单体接枝率,最高可达4%.","authors":[{"authorName":"谭秀民","id":"66350bc9-0d5f-444f-85b4-a8ce7a81895c","originalAuthorName":"谭秀民"},{"authorName":"李国强","id":"d386ded9-8ded-4c45-b6bd-8efe3f333860","originalAuthorName":"李国强"},{"authorName":"赵恒勤","id":"23761ba8-9e78-4fb2-bd20-88a256cb2d5b","originalAuthorName":"赵恒勤"}],"doi":"","fpage":"95","id":"34ff6c29-dacc-4545-b892-d1659b207136","issue":"24","journal":{"abbrevTitle":"CLDB","coverImgSrc":"journal/img/cover/CLDB.jpg","id":"8","issnPpub":"1005-023X","publisherId":"CLDB","title":"材料导报"},"keywords":[{"id":"62688b5e-9308-4727-8310-6ab172a5b56d","keyword":"微悬浮","originalKeyword":"微悬浮"},{"id":"2bebd25f-969c-41a4-a41a-7c7c65ed0ec2","keyword":"乙丙橡胶","originalKeyword":"乙丙橡胶"},{"id":"2c2d5556-12c9-429e-9b98-f9a0e2a392d9","keyword":"共辐射","originalKeyword":"共辐射"},{"id":"96074d53-55ba-4985-9e1e-45e867be9635","keyword":"马来酸酐","originalKeyword":"马来酸酐"},{"id":"1b4d04f6-d04f-457b-bf16-d1921265cdbf","keyword":"接枝","originalKeyword":"接枝"}],"language":"zh","publisherId":"cldb201024027","title":"乙丙橡胶微悬浮共辐射接枝马来酸酐","volume":"24","year":"2010"},{"abstractinfo":"使用了生物可降解的马来酸酐作为改性单体和聚乳酸(PLA)进行适当的交联,分别研究了聚乳酸和马来酸酐(MAn)的质量比为5∶1、10∶1、20∶1时材料的性质.结果发现,聚乳酸和马来酸酐的比例大于10时,材料仍然较好地保持着弹性体的性质,材料的压缩模量也得到提高,尤其在比例为10∶1时,材料压缩模量的提高更明显.","authors":[{"authorName":"曹雪波","id":"117da7e6-3009-47af-b6e0-5d9b1b8abed8","originalAuthorName":"曹雪波"},{"authorName":"王远亮","id":"1e4dec5c-125a-4c11-bf7d-a9737de643d3","originalAuthorName":"王远亮"},{"authorName":"潘君","id":"8115191d-f6fa-403f-a616-597ec1fbbc26","originalAuthorName":"潘君"},{"authorName":"卢晓","id":"cfebf45e-bc21-4fc8-99fa-af0b74607679","originalAuthorName":"卢晓"},{"authorName":"蔡绍皙","id":"65321a96-6212-47e7-86a6-4c979a708c20","originalAuthorName":"蔡绍皙"}],"doi":"","fpage":"115","id":"8383d1ca-60dc-4ef4-9a2d-d8ff6b0f3fb7","issue":"1","journal":{"abbrevTitle":"GFZCLKXYGC","coverImgSrc":"journal/img/cover/GFZCLKXYGC.jpg","id":"31","issnPpub":"1000-7555","publisherId":"GFZCLKXYGC","title":"高分子材料科学与工程"},"keywords":[{"id":"3be999b7-b32a-473b-b9cb-41727176fd63","keyword":"聚乳酸","originalKeyword":"聚乳酸"},{"id":"633a8b34-1be2-4071-bdca-804e15a4d768","keyword":"马来酸酐","originalKeyword":"马来酸酐"},{"id":"b3023077-0acd-4825-b11c-5fede08f62a9","keyword":"力学","originalKeyword":"力学"},{"id":"9d419d50-6cf5-4a1a-9f69-482d0793b3eb","keyword":"生物可降解高分 子","originalKeyword":"生物可降解高分 子"}],"language":"zh","publisherId":"gfzclkxygc200201029","title":"马来酸酐改性聚乳酸的力学性能研究","volume":"18","year":"2002"},{"abstractinfo":"采用反应挤出方法制备了聚乳酸(PLA)与马来酸酐(MAH)的接枝共聚物,研究了工艺条件和配方对产物接枝率和熔体流动速率的影响.结果表明,聚乳酸的接枝反应主要依赖于大分子侧链自由基进行,过高的螺杆转速或过高的挤出反应温度会引发聚乳酸的降解反应,不利于产物接枝率的提高;在适宜的反应条件下(马来酸酐含量2%,DCP含量0.35%.温度180℃,螺杆转速100 r/min),可以方便制得马来酸酐接枝聚乳酸产物(接枝率≥O.45%);SEM观察显示,马来酸酐接枝聚乳酸有效改善了PLA/淀粉共混材料的相容性.","authors":[{"authorName":"于人同","id":"5d769ab2-4aa1-4962-94d6-f69f0eb8938a","originalAuthorName":"于人同"},{"authorName":"方显力","id":"e4edd4ee-8953-421b-8df1-c3cd369f2530","originalAuthorName":"方显力"},{"authorName":"张云灿","id":"bf22e16c-5987-42a8-8bdf-282d15d9562e","originalAuthorName":"张云灿"},{"authorName":"陈贤益","id":"bd64b2f1-ecc2-4163-935f-c602a2055a92","originalAuthorName":"陈贤益"}],"doi":"","fpage":"85","id":"7225f86c-e17e-4f90-8e0b-6e97bd581838","issue":"3","journal":{"abbrevTitle":"GFZCLKXYGC","coverImgSrc":"journal/img/cover/GFZCLKXYGC.jpg","id":"31","issnPpub":"1000-7555","publisherId":"GFZCLKXYGC","title":"高分子材料科学与工程"},"keywords":[{"id":"1580e133-a0e5-4b53-8447-51252ae8b8a1","keyword":"聚乳酸","originalKeyword":"聚乳酸"},{"id":"eee5fcac-1c0e-4bcb-aa40-ea87f36d5046","keyword":"马来酸酐","originalKeyword":"马来酸酐"},{"id":"569a1b16-a409-4b0b-8fcd-958537ff7961","keyword":"反应挤出","originalKeyword":"反应挤出"},{"id":"9f48fb39-f6be-4a93-adf2-2be46ce98da4","keyword":"接枝","originalKeyword":"接枝"}],"language":"zh","publisherId":"gfzclkxygc200903024","title":"反应挤出法制备马来酸酐接枝聚乳酸","volume":"25","year":"2009"},{"abstractinfo":"以木质素磺酸钠(LS)、丙烯酰胺(AM)、马来酸酐(MAH)为原料,膨润土(Ben)为无机添加剂,过硫酸钾(KPS)为引发剂,N,N'亚甲基双丙烯酰胺(NMBA)为交联剂,通过溶液自由基接枝共聚法制备了膨润土/木质素磺酸钠接枝丙烯酰胺-马来酸酐(Ben/LS-g-AM-co-MAH)选择性吸附树脂.采用元素分析(EA)、比表面积和孔径分析(BET)、FTIR、核磁共振碳谱(13C NMR)、XRD、SEM-EDS及XPS对所得吸附树脂的组成与结构进行了表征.结果表明:Ben/LS-g-AM-co-MAH的结构中含有大量的酰胺基和羧基基团,其在二元Pb2+/Cu2+溶液中对Pb2+具有较高的吸附量以及良好的吸附选择性.","authors":[{"authorName":"姚庆鑫","id":"59f3c4e6-19af-4a77-9a1b-3e0573cc7bd2","originalAuthorName":"姚庆鑫"},{"authorName":"谢建军","id":"08c50acf-4b0e-49d7-88e6-b6ecbec9a9d3","originalAuthorName":"谢建军"},{"authorName":"赵玉双","id":"196148dc-9627-4da2-9bea-19d31adbeb81","originalAuthorName":"赵玉双"},{"authorName":"宋文淼","id":"08fd5b34-f388-4680-ac47-52d412e4fac7","originalAuthorName":"宋文淼"},{"authorName":"成青","id":"cfee187d-5dcc-4201-bc37-1bf2d8d42364","originalAuthorName":"成青"},{"authorName":"张平","id":"9825841c-545a-4e3b-850b-0717348acaf2","originalAuthorName":"张平"}],"doi":"10.13801/j.cnki.fhclxb.20150901.002","fpage":"797","id":"f644da7e-6ea5-42fd-ba27-c7914283cd47","issue":"4","journal":{"abbrevTitle":"FHCLXB","coverImgSrc":"journal/img/cover/FHCLXB.jpg","id":"26","issnPpub":"1000-3851","publisherId":"FHCLXB","title":"复合材料学报"},"keywords":[{"id":"806e5a0e-9c93-4265-8f68-c6f3f0c5ecad","keyword":"木质素","originalKeyword":"木质素"},{"id":"70a8ead1-f634-4610-922a-9a2c412ee5fe","keyword":"丙烯酰胺","originalKeyword":"丙烯酰胺"},{"id":"286841dd-c4f9-4ffb-95f2-ff3afd8cc1a0","keyword":"马来酸酐","originalKeyword":"马来酸酐"},{"id":"1335d792-ab31-451a-9eb7-7b157a63228f","keyword":"接枝共聚合","originalKeyword":"接枝共聚合"},{"id":"9f92d874-07ac-4da1-b433-1933f3f78d2a","keyword":"吸附树脂","originalKeyword":"吸附树脂"},{"id":"cb1fe471-3c6a-4bf4-8eab-7f914bb75cbc","keyword":"选择性吸附","originalKeyword":"选择性吸附"},{"id":"caf84bde-b5e0-4106-a2ce-8d23a554cc6e","keyword":"铅离子","originalKeyword":"铅离子"},{"id":"8003ff9c-0254-4f1c-9e2d-087c7293a4f6","keyword":"铜离子","originalKeyword":"铜离子"}],"language":"zh","publisherId":"fhclxb201604012","title":"膨润土/木质素磺酸钠-g-丙烯酰胺-马来酸酐选择性吸附树脂的制备与表征","volume":"33","year":"2016"},{"abstractinfo":"利用新型的磨盘形力化学反应器在室温下实现了马来酸酐(MAH)在聚丙烯(PP)上的固相力化学接枝.采用IR、DSC及化学滴定等方法对所制备的聚丙烯-马来酸酐接枝共聚物(PP-g-MAH)进行了分析表征.系统研究了磨盘静压力、转速、温度、、碾磨次数、聚丙烯与马来酸酐配比等因素对接枝率的影响.加入无机填料钛白粉(TiO2)共碾磨,可进一步提高MAH在PP上的接枝率.通过磨盘固相力化学反应制备的PP-g-MAH可作为PP/无机填料体系和PP/极性聚合物体系的有效的增容剂.","authors":[{"authorName":"刘才林","id":"b9232253-8ffe-423f-8343-abaa2998b374","originalAuthorName":"刘才林"},{"authorName":"王琪","id":"f5a680a5-7b47-4995-9ebb-8b4829446554","originalAuthorName":"王琪"}],"doi":"","fpage":"85","id":"7a01d8a7-f3b0-4ee3-96d5-90a16c755529","issue":"3","journal":{"abbrevTitle":"GFZCLKXYGC","coverImgSrc":"journal/img/cover/GFZCLKXYGC.jpg","id":"31","issnPpub":"1000-7555","publisherId":"GFZCLKXYGC","title":"高分子材料科学与工程"},"keywords":[{"id":"cd54f16b-5a4c-40c0-93a1-9ca32586538a","keyword":"聚丙烯","originalKeyword":"聚丙烯"},{"id":"5f787007-f409-42a2-8282-a5fd2c12e820","keyword":"固相力化学接枝","originalKeyword":"固相力化学接枝"},{"id":"e69aa544-96ef-429a-82d2-d9bb9bbf4210","keyword":"磨盘形力化学反应器","originalKeyword":"磨盘形力化学反应器"},{"id":"5f67d73c-25d7-45ea-89f1-11a4ca4341dc","keyword":"马来酸酐","originalKeyword":"马来酸酐"}],"language":"zh","publisherId":"gfzclkxygc199903025","title":"聚丙烯固相力化学接枝马来酸酐","volume":"15","year":"1999"},{"abstractinfo":"考察了马来酸酐(MAH)用量、引发剂(BPO)用量、反应温度和反应时间对氯化聚丙烯接枝马来酸酐(CPPgMAH)中接枝率和接枝效率的影响.结果表明m(MAH)∶m(CPP)=0.28时,接枝率和接枝效率较高;随着引发剂过氧化苯甲酰(BPO)用量的增大,接枝率和接枝效率也随之增大;提高反应温度,可以提高接枝效果,适宜的反应温度和反应时间分别为100 ℃、1.5 h.","authors":[{"authorName":"马向东","id":"0f80ee36-4358-415e-8793-2b08e3914141","originalAuthorName":"马向东"},{"authorName":"刘大壮","id":"d12f604e-56e4-40c8-9696-4372eb280d2a","originalAuthorName":"刘大壮"},{"authorName":"孙培勤","id":"b7c9a521-9307-4170-9dbb-1d67ac06faf8","originalAuthorName":"孙培勤"}],"doi":"10.3969/j.issn.0253-4312.2007.07.009","fpage":"29","id":"293f3df7-d30b-45c2-b064-677608b4d1d2","issue":"7","journal":{"abbrevTitle":"TLGY","coverImgSrc":"journal/img/cover/TLGY.jpg","id":"61","issnPpub":"0253-4312","publisherId":"TLGY","title":"涂料工业 "},"keywords":[{"id":"299100db-4db2-4ad8-b005-ae8d3bcff5af","keyword":"氯化聚丙烯","originalKeyword":"氯化聚丙烯"},{"id":"c87fa346-81a8-488b-8d28-ba67f375d7d2","keyword":"马来酸酐","originalKeyword":"马来酸酐"},{"id":"d7583ab3-02ef-4207-9609-96d82fd597a6","keyword":"接枝","originalKeyword":"接枝"},{"id":"6d696f70-0350-44f7-b8f4-38326586feed","keyword":"红外光谱","originalKeyword":"红外光谱"}],"language":"zh","publisherId":"tlgy200707009","title":"氯化聚丙烯接枝马来酸酐的合成研究","volume":"37","year":"2007"},{"abstractinfo":"分析了马来酸酐(MAH)不同掺量对SBS改性沥青微观结构和性能的影响.结果表明,随MAH掺量的增加,SBS改性沥青的软化点和针入度指数PI提高,但5℃延度降低.而改性沥青离析软化点差随MAH掺量增加,先减小后增大,表明相容性先改善后变差.","authors":[{"authorName":"黄锦华","id":"5588ad53-254d-4f91-9eb5-531b294c6cd8","originalAuthorName":"黄锦华"},{"authorName":"陈守明","id":"2feaa0a9-cba7-4b47-ba11-dc1f64187582","originalAuthorName":"陈守明"},{"authorName":"陈伟三","id":"9262da1d-40ba-4e9a-8884-8483054b3539","originalAuthorName":"陈伟三"}],"doi":"","fpage":"25","id":"9f8329d7-9d2c-4c68-a446-ccd1f8f3e50f","issue":"4","journal":{"abbrevTitle":"HCCLLHYYY","coverImgSrc":"journal/img/cover/HCCLLHYYY.jpg","id":"42","issnPpub":"1671-5381","publisherId":"HCCLLHYYY","title":"合成材料老化与应用"},"keywords":[{"id":"be603856-d076-4986-9dbf-2e5ab6daf4ca","keyword":"马来酸酐","originalKeyword":"马来酸酐"},{"id":"afe0e659-e42b-4057-8df6-e4f83652e7e2","keyword":"SBS改性沥青","originalKeyword":"SBS改性沥青"},{"id":"404fdd92-ed31-47be-b751-9178ddc4e323","keyword":"相容性","originalKeyword":"相容性"},{"id":"139367c8-bcaa-491d-ad0e-192a0716131b","keyword":"性能分析","originalKeyword":"性能分析"}],"language":"zh","publisherId":"hccllhyyy201304007","title":"马来酸酐对SBS改性沥青的性能影响","volume":"42","year":"2013"}],"totalpage":130,"totalrecord":1294}