TiCl3饱和NaCl溶液中采用外加添加剂尿素的新技术,于一定条件下用水热法在玻璃基板上制备出大面积TiO2纳米棒阵列薄膜.研究了尿素含量、反应温度、反应时间和TiCl3起始浓度对产物的影响,并讨论了反应机理.
参考文献
| [1] | Song C X;Wang D B;Gu G H et al.Preparation and characterization of silver/TiO2 composite hollow spheres[J].Journal of Colloid and Interface Science,2004,272:340. |
| [2] | Chen K Y;Chen Y W .Preparation of barium titanate ultrafine particles from rutile titania by a hydrothermal conversion[J].Powder Techn,2004,141:69. |
| [3] | Blesic M D;Saponjic Z V;Nedeljkovic J M et al.TiO2 films prepared by ultrasonic spray pyrolysis of nanosize precursor[J].Materials Letters,2002,54:298. |
| [4] | Zhang J;Wang B J;Ju X et al.New observations on the optical properties of PPV/TiO2 nanocomposites[J].Polymer,2001,42:3697. |
| [5] | Gundiah G;Rao C N R .Macroporous oxide materials with three-dimensionally interconnected pores[J].Solid State Sciences,2000,2:877. |
| [6] | Holgado M.;Ibisate M.;Serna CJ.;Lopez C.;Meseguer F.;Cintas A. .Three-dimensional arrays formed by monodisperse TiO2 coated on SiO2 spheres[J].Journal of Colloid and Interface Science,2000(1):6-11. |
| [7] | Maira A.J.;Yeung K.L.;Lee C.Y.;Yue P.L. .Size Effects in Gas-Phase Photo-oxidation of Trichloroethylene Using Nanometer-Sized TiO_2 Catalysts[J].Journal of Catalysis,2000(1):185-196. |
| [8] | Huisman CL;Schoonman J;Goossens A .The application of inverse titania opals in nanostructured solar cells[J].Solar Energy Materials and Solar Cells: An International Journal Devoted to Photovoltaic, Photothermal, and Photochemical Solar Energy Conversion,2005(1):115-124. |
| [9] | Yamabi S;Imai H .Synthesis of rutile and anatase films with high surface areas in aqueous solutions containing urea[J].Thin Solid Films,2003,434:86. |
| [10] | Paolo Bertoncello;Andrea Notargiacomo;Claudio Nicolini .Langmuir-Schaefer Films of Nafion with Incorporated TiO_2 Nanoparticles[J].Langmuir: The ACS Journal of Surfaces and Colloids,2005(1):172-177. |
| [11] | Ho WK;Yu JC;Yu JG .Photocatalytic TiO2/glass nanoflake array films[J].Langmuir: The ACS Journal of Surfaces and Colloids,2005(8):3486-3492. |
| [12] | Liu K;Fu H;Shi K et al.Preparation of large-pore mesoporous nanocrystalline TiO2 thin films with tailored pore diameters[J].Journal of Physical Chemistry B,2005,109(40):18719. |
| [13] | Zhengrong R. Tian;James A. Voigt;Jun Liu;Bonnie Mckenzie;Huifang Xu .Large Oriented Arrays and Continuous Films of TiO_2-Based Nanotubes[J].Journal of the American Chemical Society,2003(41):12384-12385. |
| [14] | Hosono E;Fujihara S;Kakiuchi K et al.Growth of submicrometer-scale rectangular parallelepiped rutile TiO2 films in aqueous TiCl3 solutions under hydrothermal conditions[J].Journal of the American Chemical Society,2004,126(25):7790. |
| [15] | Niesen T P;DeGuire M R J .Deposition of ceramic thin films at low temperatures from aqueous solutions[J].Journal of Electroceramics,2001,6(03):169. |
| [16] | Ki Chang Song;Yong Kang .Preparation of high surface area tin oxide powders by a homogeneous precipitation method[J].Materials Letters,2000(5):283-289. |
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