以Ti6Al4V钛合金为基体材料,通过微弧氧化方法在电解液中制备多孔氧化锆和羟基磷灰石复合医用钛合金陶瓷膜层.利用能谱分析仪、扫描电镜和X-射线衍射仪分析膜层结构及相组成特点.对试样断裂韧性进行测量试验,通过测试结果对膜层断裂韧性进行了分析研究.探究了氧化锆对于钛合金羟基磷灰石膜层的增韧机制,并建立了适于多孔微裂纹膜层材料断裂韧性数学模型.结果表明,ZrO2/羟基磷灰石医用钛合金复合陶瓷膜层比单一的羟基磷灰石陶瓷膜层具有更好的断裂韧性.
参考文献
[1] | Mcpherson R;Gane N;Bastow T .Structural characterization of plasma sprayed hydroxyapatite coatings[J].Journal of Materials Science:Materials in Medicine,1995,6(06):327-334. |
[2] | Brown S;Turner I;Reiter H .Residual stress measurement in thermal sprayed hydroxyapatite coatings[J].Journal of Materials Science:Materials in Medicine,1994,5(09):756-759. |
[3] | Mendes SC;Reis RL;Bovell YP;Cunha AM;van-Blitterswijk CA;de-Bruijn JD .Biocompatibility testing of novel starch-based materials with potential application in orthopaedic surgery: a preliminary study.[J].Biomaterials,2001(14):2057-2064. |
[4] | 李慕勤,孟祥才,庄明辉,曲立杰.热处理对钛-生物玻璃涂层结合强度的影响[J].材料热处理学报,2009(02):158-161. |
[5] | Ishizawa H;Ogino M .Formation and characterization of anodic titanium oxide films containing Ca and P.[J].Journal of biomedical materials research, Part B. Applied biomaterials,1995(1):65-72. |
[6] | A. L. Yerokhin;X. Nie;A. Leyland;A. Matthews;S. J. Dowey .Plasma electrolysis for surface engineering[J].Surface & Coatings Technology,1999(2/3):73-93. |
[7] | Sul YT .The significance of the surface properties of oxidized titanium to the bone response: special emphasis on potential biochemical bonding of oxidized titanium implant.[J].Biomaterials,2003(22):3893-3907. |
[8] | 朱瑞富,王志刚,王爱娟,肖桂勇,吕宇鹏,李士同,塙隆夫.纯钛表面微弧氧化多孔陶瓷膜的结构特性[J].材料热处理学报,2009(02):129-133. |
[9] | 李夕金,程国安,薛文斌,郑瑞廷,吴晓玲,程云君.TiAl合金微弧氧化膜的制备及抗氧化性能研究[J].材料热处理学报,2006(05):95-99. |
[10] | Son W W;Zhu X;Shin H I et al.In vivo histological response to anodized and anodized/hydrothermally treated titanium implants[J].Journal of Biomedical Materials Research Part B:Applied Biomaterials,2003,66B(02):520-525. |
[11] | Li LH;Kong YM;Kim HW;Kim YW;Kim HE;Heo SJ;Koak JY .Improved biological performance of Ti implants due to surface modification by micro-arc oxidation.[J].Biomaterials,2004(14):2867-2875. |
[12] | 杨延清,罗贤,黄斌,李建康,陈彦.SiCf/Ti-6Al-4V复合材料的断裂韧性[J].材料热处理学报,2010(09):1-4. |
[13] | 黄勇;汪长安.高性能多相复合陶瓷[M].北京:清华大学出版社,2008:134-136. |
[14] | 阮建明;邹俭鹏;黄伯云.生物材料学[M].北京:科学出版社,2004:73-89. |
[15] | F. Tancret;J.-M. Bouler;J. Chamousset .Modelling the mechanical properties of microporous and macroporous biphasic calcium phosphate bioceramics[J].Journal of the European Ceramic Society,2006(16):3647-3656. |
[16] | F. Pecqueux;F. Tancret;N. Payraudeau .Influence of microporosity and macroporosity on the mechanical properties of biphasic calcium phosphate bioceramics:Modelling and experiment[J].Journal of the European Ceramic Society,2010(4):819-829. |
[17] | 郑立允,王玉果,赵立新,张京军,熊惟皓.TiN/TiAIN涂层的断裂韧性研究[J].稀有金属材料与工程,2008(z1):752-755. |
[18] | 詹世革;王自强;韩学礼 .二维多裂纹弹性体的有效弹性模量[J].中国科学a辑,1998,8(28):751-756. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%