Fe3O4亚微米球的水热制备及表征

人工晶体学报, 2008, 37(6): 1514-1517.

Fe3O4亚微米球的水热制备及表征

胡林 ^1, , 张元广 ^2, , 赵英国 ^3, , 陈友存 ^4,

1.安庆师范学院化学系,安庆,246011

2.安庆师范学院化学系,安庆,246011

3.安庆师范学院化学系,安庆,246011

4.安庆师范学院化学系,安庆,246011

基金项目: 安徽省教育厅自然科学基金(2006kj042A) 国家自然科学基金(20371002;20771006)

关键词： Fe3O4 , 亚微米球 , 水热制备 , 表征

Hydrothermal Preparation and Characterization of Fe3O4 Submicrospheres

以FeSO4·7H2O和 KNO3为前驱物,在KOH溶液中,160 ℃水热反应15 h,成功合成了立方相的Fe3O4亚微米球.初步探索了反应温度和反应时间对合成产物的影响.利用X射线粉末衍射(XRD),透射电子显微镜(TEM)和高分辨透射电子显微镜(HRTEM)等手段对产物进行了表征.结果表明,产物为立方结构的Fe3O4纯相,呈现球状形貌.该亚微米球的平均粒径约为350 nm,内部具有精细结构,是由粒径更小的Fe3O4单晶颗粒组成.

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材料期刊网

Fe3O4亚微米球的水热制备及表征

Hydrothermal Preparation and Characterization of Fe3O4 Submicrospheres

参考文献