研究了以硝酸锂、硝酸铝和尿素为原料,用溶胶-凝胶燃烧合成法制备γ-LiAlO2粉体的工艺.采用热重分析(TG-DTA)、X射线衍射(XRD)、红外光谱(IR)、扫描电镜(SEM)对反应前驱体、反应过程、燃烧产物进行了表征测试.分析了原料配比、溶胶前驱体pH值对反应产物特性的影响,并初步探讨了反应的历程.
参考文献
| [1] | 陈铭,温廷琏.LiAlO2粉体的合成[J].化学通报,1998(10):19-23. |
| [2] | 陈刚,付拥峰,胡克鳌,张荻.电解质基板材料γ-LiAlO2粉体的合成制备[J].上海交通大学学报,2003(02):260-263. |
| [3] | 高志强,沈晓冬,崔升,肖苏.纳米铝酸锂粉体制备方法的研究[J].材料导报,2006(z2):145-148. |
| [4] | 许前丰,严有为.前驱体溶液配比及pH值对凝胶-燃烧合成纳米MgO颗粒的影响[J].功能材料,2006(03):392-394. |
| [5] | 殷声.燃烧合成[M].北京:冶金工业出版社,1999 |
| [6] | 李汶霞,殷声.低温燃烧合成陶瓷微粉[J].硅酸盐学报,1999(01):70-78. |
| [7] | Jain SR;Adiga K C .A new approach to thermochemical calculations of condensed fuel-oxidizer mixtures[J].Combustion and Flame,1981,40(01):71. |
| [8] | Zhang Y;Strangle G C .Preparation of fine multicomponent oxide ceramic power by a combustion synthesis proeess[J].Journal of Materials Research,1994,9(08):1997. |
| [9] | 李飞,胡克鳌,张栋.燃烧合成制备γ-偏铝酸锂粉体[J].材料科学与工程,2002(03):313-316. |
| [10] | Ribeiro RA.;Mohallem NDS.;Silva GG. .The influences of heat treatment on the structural properties of lithium aluminates[J].The journal of physics and chemistry of solids,2001(5):857-864. |
| [11] | Chatterjee M;Naskar M K .Novel technique for synthesis of lithium aluminate(LiAlO2)powders from water-based sols[J].Journal of Materials Science Letters,2003,22(24):1747. |
| [12] | 沈彩,刘庆峰,刘茜.柠檬酸-硝酸盐燃烧法制备Ba0.5Sr0.5TiO3介电材料[J].无机材料学报,2004(03):681-685. |
| [13] | 李飞,胡克鳌,李建林,张栋,吴桢干.凝胶燃烧法合成LiCoO2超细粉体的研究[J].金属学报,2002(02):140-144. |
| [14] | SANG WOON KWON;SEUNG BIN PARK .Effect of precursors on the morphology of lithium aluminate prepared by hydrothermal treatment[J].Journal of Materials Science,2000(8):1973-1978. |
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