介绍了一种新型气体吸附测量装置. 该装置利用压差法测量,采用美国MKS高精度压差传感器来提高测量精度,通过微调泄漏阀控制极小进气量,并且采用间断法与连续法相结合. 实验证明,该装置具有很好的可重复性,能获得高分辨率及超低压吸附等温线.
参考文献
[1] | Gregg S J;Sing K S W.Adsorption,Surface Area and Porosity[M].London:Academic Press,1982:41. |
[2] | Rouquerol F;Rouquerol J;Sing K S W.Adsorption by Powders and Porous Solids[M].London:Academic Press,1999 |
[3] | Anderson J R;Pratt K C.Introduction to the Characterization and Testing of Catalysts[M].London:Academic Press,1985:1. |
[4] | Chen S Y;Sun Y H;Ding Y J;Zhou R X,Luo M F.Adsorption and Catalysis[M].郑州:河南科学技术大学,2001:1. |
[5] | 李林,王晓东,沈俭一,周立幸,张涛.高灵敏宽温区吸附热测定装置的建立[J].催化学报,2003(11):872-876. |
[6] | Innes W B .[J].Analytical Chemistry,1951,23(05):759. |
[7] | Lange K R .[J].Journal of Colloid Science,1963,18(01):65. |
[8] | Pieters W J M;Gates W E .[P].US 4489593,1984. |
[9] | Ito M;Abe T;Orii R;Yamakoshi T .[P].US 5109716,1992. |
[10] | Rouquerol J;Davy L J .[P].US 4967591,1990. |
[11] | Ajot H;Joly J F;Garnier D A;Marny F,Raatz F,Russmann C .[P].US 5239482,1993. |
[12] | Borghard W S;Schoennagel H J .[P].US 4762010,1988. |
[13] | Conner C W;Fraissard J;Conner C W.Physical Adsorption:Experiment,Theory and Applications[M].Boston:Kluwer Academic Publishers,1997:33. |
[14] | Zhou J P;Yu Ch Ch;Shen Sh K .[J].Fenxi Ceshi Jishu Yuyiqi (Anal Test Technol Instrum),1999,5(02):85. |
[15] | Wang D Z;Wei F;Wang J F .[P].CN 200310113533,2004. |
[16] | Li FX;Wang Y;Wang DZ;Wei F .Characterization of single-wall carbon nanotubes by N-2 adsorption[J].Carbon: An International Journal Sponsored by the American Carbon Society,2004(12/12):2375-2383. |
[17] | Cejka J;Zilkova N;Rathousky J;Zukal A;Jagiello J .High-resolution adsorption of nitrogen on mesoporous alumina[J].Langmuir: The ACS Journal of Surfaces and Colloids,2004(18):7532-7539. |
[18] | Villieras F.;Charmas B.;Bardot F.;Gerard G.;Rudzinski W.;Leboda R. .High resolution argon and nitrogen adsorption assessment of the surface heterogeneity of carbosils[J].Carbon: An International Journal Sponsored by the American Carbon Society,1998(10):1501-1510. |
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