采用溶胶-凝胶法合成Al掺杂ZnO胶体,通过浸涂法在石英衬底上制备不同退火温度的ZAO薄膜.通过XRD、FT-IR、IR-2型红外辐射仪等手段对薄膜进行表征并研究不同工艺条件对薄膜红外性能的影响.结果显示,Al的掺杂并未改变ZnO的晶型结构,薄膜材料具有沿(002)晶面趋向性生长的特点.ZAO薄膜在可见光区具有高透过率,平均透过率在80%左右,在红外波段具有较高的透过率,所得到的ZAO薄膜在红外波段具有较低的发射率.
Al-doped ZnO(ZAO)thin film was deposited on quartz glass by sol-gel process with different sintering temperatures. The infrared characters and the effect of technics were investigated through X-ray diffraction (XRD), FT-IR and IR-2 infrared actinograph. The XRD results show that the phase structure of ZAO thin films was the same as that of ZnO with highly C-axis oriented. The FT-IR results show that ZAO thin films had a high transparence ( about 80% ) for visible light and a high transparence for infrared.The ZAO thin films take a low infrared emissivity.
参考文献
[1] | 王银铃;徐雪青;徐刚 et al.[J].材料导报,2008,22(02):297. |
[2] | 王涛,刁训刚,丁芃,舒远杰,武哲.磁控溅射低温制备ZnO∶Al透明导电膜及其特性研究[J].真空科学与技术学报,2007(06):511-516. |
[3] | 孙福来;谭红琳 .[J].功能材料,2007,38:824. |
[4] | 刁训刚,郝维昌,王天民,武哲,黄俊.低发射率薄膜的红外隐身特性研究[J].宇航材料工艺,2007(05):39-42. |
[5] | 刘耀东;范伟光;谷立娟 .[J].稀有金属材料与工程,2007,36(Suppl 3):340. |
[6] | Schuler T;Aegerter M A .[J].Thin Solid Films,1999,351:125. |
[7] | Myong S Y;Baik S J;Lee C H.[J].Journal of Applied Physics,1997(36):68. |
[8] | Atsushi Sasaki;Wakana Hara;Akifumi Matsuda et al.[J].Applied Physics Letters,2005,86(23):911. |
[9] | 岳春晓,姚兰芳,汪国庆,鲁凤芹,关飞飞,谢伏将.ZAO纳米粉体的制备及其在红外隐身中的应用研究[J].材料导报,2008(z1):139-141. |
[10] | 郝雷,刁训刚,顾宝霞,王天民.红外可见兼容隐身薄膜的制备与性能[J].宇航材料工艺,2008(02):26-29. |
[11] | 薛文书;祖小涛;陈美艳 et al.[J].强激光与粒子束,2007,19(01):142. |
[12] | 胡传炘.隐身涂层技术[M].北京:化学工业出版社,2004:121. |
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