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采用磁场-电沉积方法在40Cr钢表面制得Ni-TiN复合镀层.利用扫描电镜(SEM)、显微硬度计、X射线衍射仪(XRD)及磨损试验机等对Ni-TiN镀层的表面形貌、显微硬度、织构和耐磨性能进行研究.结果表明,脉冲占空比为50%时,镀层表面镍晶粒平均粒径65.3 nm,且镀层中TiN粒子复合量较多.随着脉冲占空比的增加,Ni-TiN镀层的显微硬度先增加后降低.脉冲占空比为50%时,Ni-TiN镀层的显微硬度达到最大值934 Hv,其磨损量和平均摩擦系数分别为28.5 mg和0.43.

参考文献

[1] 兰宏宇;马春阳;李洋;夏法锋.电沉积工艺参数对Ni-TiN纳米复合镀层粒子复合量的影响[J].兵器材料科学与工程,2015(3):52-54.
[2] F.F. Xia;C. Liu;F. Wang.Preparation and characterization of Nano Ni-TiN coatings deposited by ultrasonic electrodeposition[J].Journal of Alloys and Compounds: An Interdisciplinary Journal of Materials Science and Solid-state Chemistry and Physics,20101/2(1/2):431-435.
[3] Chunyang Ma;Guiqiang Liang;Yongyong Zhu.Preparation and corrosion assessment of electrodeposited Ni-SiC composite thin films[J].CERAMICS INTERNATIONAL,20142(2):3341-3346.
[4] Xingyuan Li;Yongyong Zhu;Guorong Xiao.Application of artificial neural networks to predict sliding wear resistance of Ni-TiN nanocomposite coatings deposited by pulse electrodeposition[J].CERAMICS INTERNATIONAL,20148 Pt.A(8 Pt.A):11767-11772.
[5] Fafeng Xia;Chao Liu;Chunhua Ma.Preparation and corrosion behavior of electrodeposited Ni-TiN composite coatings[J].International Journal of Refractory Metals & Hard Materials,2012Nov(Nov):295-299.
[6] Xia, FF;Wu, MH;Wang, F;Jia, ZY;Wang, AL.Nanocomposite Ni-TiN coatings prepared by ultrasonic electrodeposition[J].Current applied physics: the official journal of the Korean Physical Society,20091(1):44-47.
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