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为了开发一种成本低廉、环境友好且镀层性能好的化学镀铜工艺,以草酸电解还原溶液为还原剂在A3钢表面进行化学镀铜。探讨了镀液组成、pH值及温度对镀铜速度、镀液稳定性及镀层附着力的影响。结果表明:最佳工艺为12~15g/L CuSO4,30~40g/LEDTA,10~20mg/L2,2’-联吡啶,10~12g/L乙醛酸+5—7g/L草酸(草酸电解还原溶液),pH=12,温度50℃,时间30min;所得镀层附着力良好,外观均匀光亮,镀速达2.2μm/,h,且镀液稳定。本工艺无污染、成本低,为化学镀铜提供了一种新的绿色环保工艺。

参考文献

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