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通过XRD、SEM、EDS等方法,研究了添加Y2O3和Sm2O3的α-Sialon-AlN-多型体复相组份在热压过程中的致密化、相组成及微观结构的变化.结果表明,复相Sialon组份,AlN-多型体先于α-Sialon形成,且易发生偏聚,很难均匀分散在α-Sialon中,但是与通常不一样,α-Sialon易发育成长颗粒状.文中对长颗粒状的α-Sialon的形成进行了讨论.

The densification behavior, reaction sequence and microstructural development of (Y+Sm) α -AlN-polytypoids multi-phase Sialon were studied by XRD, SEM and EDS. The results show that the AlN-polytypoids form earlier than α-Sialon and segregate together. The α-Sialon develops into elongated grains in this multi-phase Sialon. The mechanism of elongated α-Sialondeveloped was discussed.

参考文献

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[4] Li H X, Sun W Y, Yan D S, et al. In: Yan D S, et al, ed. Proc. 5th Inter. Sym. on ceramic materials &
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