欢迎登录材料期刊网

材料期刊网

高级检索

采用溶胶-凝胶法在LaAlO3(LAO)单晶衬底上制备了Zn^2+掺杂的YBCO薄膜,用X射线衍射(XRD)、高分辨透射电子显微镜(HRTEM)以及标准四引线法分别研究了Zn^2+掺杂的YBCO薄膜的微观结构、生长取向以及超导性能。结果表明,随Zn2+掺杂浓度的增大薄膜的临界电流密度提高,而临界转变温度下降、临界转变温区变宽;但当掺杂量〉0.5%(摩尔分数)时,会影响YBCO的c轴取向生长,导致超导性能变差。通过优化掺杂比例后得到Zn2+掺杂0.5%(摩尔分数)的YBCO薄膜具有最好的综合超导性能,其TC为91.3K,ΔT为1.1K,Jc约为1.54MA/cm^2(77K,0T)。

Zn2+-doped YBCO thin films were prepared on LaAlO3(LAO) single-crystal substrates by sol-gel process.The microstructure and growth orientation of the Zn2+-doped YBCO thin films were analyzed by X-ray diffraction(XRD) and transmission electron microscopy(TEM) respectively.The standard four-probe method was used to measure the superconducting properties of the pure and doped YBCO thin films.The results show that the critical current density Jc of the Zn^2+-doped YBCO films was improved with the increase of Zn2+ concentration,although critical transition temperature TC was decreased and transition width ΔT was broadened.When the Zn^2+ doping percentage is over 0.5mol%,the YBCO films exhibit deteriorated superconducting properties due to bad c-axis growth orientation.It is found that YBCO film doped with 0.5mol% Zn^2+ show the best superconducting performance with TC of 91.3K,ΔT of 1.1K and Jc of 1.54MA/cm2(77K,0T).

参考文献

[1] Fu LF;Browning ND;Ramadan W;Ogale SB;Kundaliya DC;Venkatesan T .Interface and defect structures in YBa2Cu3O7-delta and Nb : SrTiO3 heterojunction[J].Journal of Physics, D. Applied Physics: A Europhysics Journal,2007(26):187-191.
[2] Hussain, M;Takita, K .Improved critical current density in Zn doped YBCO single crystals[J].Physica, C. Superconductivity and its applications,2010(4):291-294.
[3] Masui T;Takano Y;Yoshida K;Kajita K;Tajima S .The effect of Zn-substitution and carrier doping on vortex pinning in YBa2Cu3O7-delta single crystals[J].Physica, C. Superconductivity and its applications,2004(Pt.2):515-520.
[4] Gaoyang Zhao;Yuanqing Chen;Li Lei;Renzhong Xue .Fabrication of <SPAN class=roman>YBa</SPAN><SUB>2</SUB><SPAN class=roman>Cu</SPAN><SUB>3</SUB><SPAN class=roman>O</SPAN><SUB>7?<SPAN class=roman>x</SPAN></SUB> Superconducting Films Using Low-Fluorine-Content Solutio[J].IEEE Transactions on Applied Superconductivity: A Publication of the IEEE Superconductivity Committee,2007(1):40-43.
[5] 张黄莉,赵高扬,彭海军.溶胶-凝胶法制备YBCO超导薄膜微细图形[J].无机材料学报,2009(01):192-194.
上一张 下一张
上一张 下一张
计量
  • 下载量()
  • 访问量()
文章评分
  • 您的评分:
  • 1
    0%
  • 2
    0%
  • 3
    0%
  • 4
    0%
  • 5
    0%