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采用低温快速热压法原位反应制备了微-纳米Al2O3原位增强Fe-Cr-Ni金属基复合材料.研究了烧结温度和保温时间对复合材料微观组织和力学性能的影响.XRD分析表明在烧结温度为700℃和800℃时,生成产物为(fcc)Cr0.19Fe0.7Ni0.11,(fcc)Fe-cr和Al2O3;SEM分析显示烧结温度为800℃,保温时间为1 h时晶粒分布更均匀,形成更致密的网状结构并且断裂形式为穿晶断裂和沿晶断裂;TEM分析得出微-纳米Al2O3颗粒为晶间型和晶内型复合.通过调节烧结温度和保温时间,制备了力学性能优良的微.纳米Al2O3原位增强Fe-Cr-Ni金属基复合材料.

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