对含铌及Nb-Ti铁素体不锈钢进行固溶和高温时效处理,采用高温拉伸试验对其进行高温力学测试.结果表明:随着时效时间的延长,铌钢高温屈服强度降低较快,而Nb-Ti钢高温屈服强度变化不大.采用相分析、扫描电镜、透射电镜对固溶铌及微观结构进行分析,发现时效过程中固溶铌含量均降低,含铌及Nb-Ti钢500h时效后固溶铌相差不大,铌钢中析出相主要是NbN相和M6C相(Fe3Nb3C),Ti-Nb钢主要析出相是NbTi(C,N)相和Laves相(Fe2Nb).长时间时效后,M6C相和Laves相严重粗化且分布变化明显.M6C相粗化后观察不到沿晶界连续分布,而Laves相粗化后主要在晶界连续分布,起到强化晶界的作用.
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