采用胶体化学法,以氧化钨(W18O49)为钨源制备出花状硒化钨纳米晶.采用透射电子显微镜(TEM)、高分辨透射电镜(HRTEM)和X射线衍射(XRD)手段对硒化钨纳米晶进行表征.本文对硒化钨花状纳米晶体的可控合成进行了初步探索,同时对烧结后的硒化钨纳米晶进行了电催化产氢测试.结果表明,硒化钨花状纳米晶具有良好的电催化性能.
参考文献
[1] | Dasgupta, N.P.;Liu, C.;Andrews, S.;Prinz, F.B.;Yang, P..Atomic layer deposition of platinum catalysts on nanowire surfaces for photoelectrochemical water reduction[J].Journal of the American Chemical Society,201335(35):12932-12935. |
[2] | Ambrosi, Adriano;Sofer, Zdenek;Pumera, Martin.2H -> 1T phase transition and hydrogen evolution activity of MoS2, MoSe2, WS2 and WSe2 strongly depends on the MX2 composition[J].Chemical communications,201540(40):8450-8453. |
[3] | Berit Hinnemann;Poul Georg Moses;Jacob Bonde;Kristina P.Jorgensen;Jane H.Nielsen;Sebastian Horch;Ib Chorkendorff;Jens K.Norskov.Biomimetic Hydrogen Evolution:MoS_2 Nanoparticles as Catalyst for Hydrogen Evolution[J].Journal of the American Chemical Society,200515(15):5308-5309. |
[4] | Jaramillo TF;Jorgensen KP;Bonde J;Nielsen JH;Horch S;Chorkendorff I.Identification of active edge sites for electrochemical H-2 evolution from MoS2 nanocatalysts[J].Science,20075834(5834):100-102. |
[5] | Ya Yan;BaoYu Xia;Xiaoming Ge.Ultrathin MoS2 Nanoplates with Rich Active Sites as Highly Efficient Catalyst for Hydrogen Evolution[J].ACS applied materials & interfaces,201324(24):12794-12798. |
[6] | Junfeng Xie;Jiajia Zhang;Shuang Li;Fabian Grote;Xiaodong Zhang;Hao Zhang;Ruoxing Wang;Yong Lei;Bicai Pan;Yi Xie.Controllable Disorder Engineering in Oxygen-Incorporated MoS_2 Ultrathin Nanosheets for Efficient Hydrogen Evolution[J].Journal of the American Chemical Society,201347(47):17881-17888. |
[7] | Li XL.;Liu JF.;Li YD..Large-scale synthesis of tungsten oxide nanowires with high aspect ratio[J].Inorganic Chemistry: A Research Journal that Includes Bioinorganic, Catalytic, Organometallic, Solid-State, and Synthetic Chemistry and Reaction Dynamics,20033(3):921-924. |
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