采用层层自组装的方法,把多金属氧酸盐PMo12O4003-和与Cu2+络合的聚酰胺-胺树形分子PAMAM(PAMAM-Cu2+)交替吸附成膜.X射线光电子能谱(XPS)、紫外可见光谱(UV-Vis)、原子力显微镜(AFM)和循环伏安法(CV)测试表明,PMo12O403-和PAMAM-Cu2+能通过静电作用形成多层膜且膜的增长均一稳定,该多层膜修饰电极对H2O2和NO2有较好的电催化还原活性.
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