采用在常规模压生坯中浸渗Al的方法,研究了MoSi2+Mo反应熔渗Al后的显微组织和力学性能的变化情况.研究表明:MoSi2坯体在1350℃反应浸渗Al可使抗弯强度高达737 MPa,其断裂韧性也可达到4.3 MPa·m1/2,远远高于热压单相材料;然而其相成分中存在残余的Si相和Al相将会阻碍其高温应用;在MoSi2坯体中加入Mo粉可以消除残余硅相;经过计算,当Mo添加量为15%(质量分数,下同)时,可以完全消除Si相,并使Al相达到最低,而其强度并不降低.同时SEM观察表明,添加15%Mo后其断口显示晶粒间絮状夹层变成颗粒状:黑色相面积较未加入Mo粉时减小.从而进一步证实添加15%Mo产生的组织变化将有利于该材料的高温力学性能.
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