Cu films with thickness of 630-1300nm were deposited on glass substrates withoutheating by DC magnetron sputtering in pure Ar gas. Ar pressure was controlled to0.5, 1.0 and 1.5Pa respectively. The target voltage was fixed at 500V but the targetcurrent increased from 200 to 1150mA with Ar pressure increasing. X-ray diffrac-tion, scanning electron microscopy and atomic force microscopy were used to observethe structural characterization of the films. The resistivity of the films was measuredusing four-point probe technique. At all the Ar pressures, the Cu films have mixturecrystalline orientations of [111], [200] and [220] in the direction of the film growth.The film deposited at lower pressure shows more [111] orientation while that depositedat higher pressure has more [220] orientation. The amount of larger grains in the filmprepared at 0.5Pa Ar pressure is slightly less than that prepared at 1. 0Pa and 1.5PaAr pressures. The resistivities of the films prepared at three different Ar pressures rep-resent few differences, about 3-4 times of that of bulk material. Besides the depositionrate increases with Ar pressure because of the increase in target current. The contri-bution of the bombardment of energetic reflected Argon atoms to these phenomena isdiscussed.
参考文献
[1] | H S Kim;Y W Oh;J S Song;B K Min .[J].Journal of Magnetism and Magnetic Materials,1998,177-181:907. |
[2] | HQiu;Y Zhang;Y R Ren .[P].中国专利 Application:001093339,2000. |
[3] | C S Liu;L J Chen .[J].Applied Surface Science,1996,92:84. |
[4] | J A Thronton .[J].Journal of Vacuum Science and Technology,1986(A4):3059. |
[5] | J A Thronton;D W Hoffman .[J].Journal of Vacuum Science and Technology,1982(20):355. |
[6] | HQiu;F P Wang;P Wu;L Q Pan Y Tian.Proc of 6th Inter Symp Sputtering and PlasmaProcesses[C].Kanazawa,Japan,2001:135. |
[7] | K. Sumi;H. Qiu;H. Kamei;S. Moriya;M. Murai;M. Shimada;T. Nishiwaki;K. Takei;M. Hashimoto .Structural, compositional and piezoelectric properties of the sol-gel Pb(Zr_(0.56)Ti_(0.44))_(0.80)(Mg_(1/3)Nb_(2/3))_(0.20)O_3/Pb(Zr_(0.56)Ti_(0.44))O_3 composite films[J].Thin Solid Films: An International Journal on the Science and Technology of Thin and Thick Films,1999(12):270-275. |
[8] | R S Robinson .[J].Journal of Vacuum Science and Technology,1979(16):185. |
[9] | J M E Harper;J J Cuomo;R J Gambino;H R Kaufman,R S Robinson .[J].Journal of Vacuum Science and Technology,1978(15):1597. |
[10] | C Hudson;R E Somekh .[J].Journal of Vacuum Science and Technology A,1996,a14:2169. |
[11] | R E Somekh .[J].真空,1984,34:987. |
[12] | D M Mattox .[J].Journal of Vacuum Science and Technology,1989,A7:1105. |
[13] | F Reniers;M P Delplancke;A Asskali;V Rooryck,O Van Sinay .[J].Applied Surface Science,1996,92:35. |
- 下载量()
- 访问量()
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%