The formation of nonequilibrium phase by mechanical alloying (MA) of Fe and B powders in a high energy vibration ball mill has been made for Fe100-xBx system with x=15. 30, 35, 45,55 and 70. By using the X-ray diffraction, magnetic measurement and M6ssbauer spectrummethods, it was revealed that the structure of the MA product varies with milling time and B contents.
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