利用透射电镜和高分辨透射电镜(HRTEM)研究了高压扭转大塑性变形纳米结构Al-Mg合金中的位错和晶界结构.结果表明:对尺寸小于100nm的晶粒,晶内无位错,其晶界清晰平直；而尺寸大于200nm的大晶粒通常由几个亚晶或位错胞结构组成,局部位错密度可高达1017m-2,这些位错往往以位错偶和位错环的形式出现.用HRTEM观察到了小角度及大角度非平衡晶界、小角度平衡晶界和大角度∑9平衡晶界等不同的晶界结构.基于实验结果,分析了局部高密度位错、位错胞和非平衡晶界等在晶粒细化过程中的作用,提出了高压扭转Al-Mg合金的晶粒细化机制.
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