低温燃烧合成工艺结合了溶液法和高温自蔓延合成超细粉末工艺的特点,可以在较低的温度下引发化学反应,并利用反应自身的放热效应维持反应的继续进行.在硝酸盐-柠檬酸体系中用该工艺直接合成了比表面积超过120 m2/g的La0.9Sr0.1Ga0.8Mg0.2O2.85固体电解质超细粉末.研究了硝酸盐溶液起始浓度和pH值对产物性能的影响.
参考文献
[1] | ISHIHARA T;Matsuda H;Takita Y .Doped LaGaO3 Perovs-kite Type Oxide as A New Oxide Ionic Conductor[J].Journal of the American Chemical Society,1994,116:3801-3803. |
[2] | Feng M;Goodenough J B .A Superior Oxide-ion Electro-lyte[J].European Journal of Solid State and Inorganic Chemistry,1994,31:663-672. |
[3] | Huang KQ.;Goodenough JB.;Feng M. .SOL-GEL SYNTHESIS OF A NEW OXIDE-ION CONDUCTOR SR- AND MG-DOPED LAGAO3 PEROVSKITE[J].Journal of the American Ceramic Society,1996(4):1100-1104. |
[4] | Huang K;Goodenough J B .Wet Chemieal Synthesis of Sr- and Mg-doped LaGaO3, A Perovskite-type Oxide-ion Conductor[J].Journal of Solid State Chemistry,1998,136:274-283. |
[5] | 谢丹;潘伟;史慧 .Mechanism Study of Sr1-xBaxBi4Ti4O15 Ferroelectrics Materials Fabricated by Sol-gel Process[J].稀有金属材料与工程,2002,31(z1):331-334. |
[6] | 邬俊波;南军;赵淑金 et al.Preparation of LTNO Ceramics Via Sol-Gel Method and Its Thermoelectric Properties[J].稀有金属材料与工程,2002,31(z1):335-339. |
[7] | Cuneyt Tas A;Majewski P J;Aldinger Fritz .Preparation of Strontium- and Zinc-doped LaGaO3 Powders via Precipi-tation in the Presence of Urea An/or Enzyme Urease[J].Journal of the American Ceramic Society,2002,85(06):1414-1420. |
[8] | Q. X. Fu;C. R. Xia;S. W. Zha .The Key Materials Used for Reduced Temperature Ceramic Fuel Cells[J].Key engineering materials,2002(224/226):159-162. |
[9] | Stevenson JW.;Mccready DE.;Pederson IR.;Weber WJ.;Armstrong TR. .PROCESSING AND ELECTRICAL PROPERTIES OF ALKALINE EARTH-DOPED LANTHANUM GALLATE[J].Journal of the Electrochemical Society,1997(10):3613-3620. |
[10] | 李汶霞,殷声.低温燃烧合成陶瓷微粉[J].硅酸盐学报,1999(01):70-78. |
[11] | Kingsley J J;Patil K C .Anover Combustion Process for the Synthesis of Fine Particle α-alumina and Related Oxide Materials[J].Materials Letters,1988,6(11/12):427-432. |
[12] | T.V. Anuradha;S. Ranganathan;Tanu Mimani .COMBUSTION SYNTHESIS OF NANOSTRUCTURED BARIUM TITANATE[J].Scripta materialia,2001(8-9):2237-2241. |
[13] | J. Poth;R. Haberkorn .Combustion-synthesis of SrTiO_3 Part I. synthesis and properties of the ignition products[J].Journal of the European Ceramic Society,2000(6):707-713. |
[14] | Jain S R;Adiga K C .A New Approach to Thermochemical Calculations of Condensed Fuel-oxidizer Mixtures[J].Combustion and Flame,1981,40:71-79. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%