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采用热台偏光显微镜观察以ACRT+ Bridgman法获得、经过金相抛光处理的弛豫铁电PMN-32PT单晶[100]cub切型电畴组态,考察了未退火状态下[100]cub切型单晶的消光行为及连续升温对本征电畴与由抛光机械应力诱导非本征电畴组态的影响.结果表明,在升温过程中,PMN-32PT单晶非本征电畴在三方-四方铁电相变后消失;本征电畴组态的变化表现为两个阶段,第一阶段畴先细化后宽化,第二阶段进行铁电-顺电相变,相变过程缓慢,持续范围为168~177℃,且与三方-四方相变出现次序相反.

参考文献

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[3] Xi Zengzhe;Luo Hailong;Long Wei et al.The influence of element distribution on piezoelectric and dielectric properties of pMN-32PT single crystal[J].Ferroelectrics,2009,384(01):140.
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[5] Ye Z G;Dong M;Zhang L .Domain structures and phase transitions of the relaxor-based piezo/ferroelectric Pb(Zn1/3-Nb2/3)O3-0.09PbTiO3 single crystals[J].Ferroelectrisc,1999,229:223.
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[7] Peng Bao;Feng Yan;Xiaomei Lu;Jinsong Zhu;Huimin Shen;Yening Wang;Haosu Luo .Coexistence of M_(A) and M_(C) phases in Pb(Mg_(1/3)Nb_(2/3))_(0.68)Ti_(0.32)O_(3) single crystals[J].Applied physics letters,2006(9):092905-1-092905-3-0.
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