材料导报, 2012, 26(10): 36-38.
升温对[100]cub弛豫铁电PMN-32PT单晶电畴组态演变的影响
龙伟 1, , 惠增哲 2, , 李晓娟 秦学枫","id":"4a3ce18c-bb1a-43c1-b21f-262aa271a891","originalAuthorName":"秦学枫"}],"doi":"","fpage":"235","id":"5f0ac01b-a50c-40f4-9cf0-202a662d3bd1","issue":"3","journal":{"abbrevTitle":"CLRCLXB","coverImgSrc":"journal/img/cover/CLRCLXB.jpg","id":"15","issnPpub":"1009-6264","publisherId":"CLRCLXB","title":"材料热处理学报"},"keywords":[{"id":"d00ef2fe-e433-4482-b884-87ccbcce5a41","keyword":"20CrMnTiH","originalKeyword":"20CrMnTiH"},{"id":"d83ac60e-18f4-4068-bfa0-ec88b622ddf2","keyword":"晶粒长大模型","originalKeyword":"晶粒长大模型"},{"id":"ecf920d4-7609-4490-a7ff-2b27d4a9563f","keyword":"Sellars模型","originalKeyword":"Sellars模型"},{"id":"370a2e29-594f-43ab-a56c-66e1a01fa5a7","keyword":"有限元模拟","originalKeyword":"有限元模拟"}],"language":"zh","publisherId":"jsrclxb201603040","title":"20CrMnTiH钢奥氏体晶粒长大规律及有限元模拟","volume":"37","year":"2016"},{"abstractinfo":"杏枫山金矿床位于湘中白马山—龙山东西向构造带与古台山—新宁南北向构造带的交汇部位,是一典型的石英细脉带型金矿床.在研究矿区地质特征基础上,通过对矿体特征、矿石成分、成矿作用过程等分析研究,提出该矿床成矿模式.认为该矿床的形成主要经历了4个阶段:第一阶段,青白口系高涧群初始矿源层的形成；第二阶段,区域深大断裂,变质作用阶段,金元素聚集、分解、化合、氧化、还原、沉淀、再循环,形成矿化富集层；第三阶段,多次岩浆活动,成矿热液形成,断裂构造活动,形成运移通道；第四阶段,岩浆活动,旧断裂复活,新断裂产生,金富集成矿.","authors":[{"authorName":"陈武","id":"e10115ae-dafb-46b5-a11a-507d5fcd8f9d","originalAuthorName":"陈武"},{"authorName":"张寿庭","id":"1c45581a-d164-4eaf-b196-439448a3766e","originalAuthorName":"张寿庭"},{"authorName":"伦生平","id":"0f004897-ddf7-41f1-aa28-daedd2b6b727","originalAuthorName":"伦生平"}],"doi":"10.11792/hj20130205","fpage":"16","id":"9980d6cd-0f02-4999-a020-7213819003e1","issue":"2","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"a27a477a-b91b-4820-87c2-fb503e457da6","keyword":"杏枫山金矿床","originalKeyword":"杏枫山金矿床"},{"id":"3683ebfb-731d-4b05-ba8e-28d2da9ee3ab","keyword":"地质特征","originalKeyword":"地质特征"},{"id":"d4ffb169-0777-4d9a-9d9c-dec3c5a5f763","keyword":"成矿模式","originalKeyword":"成矿模式"},{"id":"e748319d-15d5-4ab9-806a-b76016d305be","keyword":"湖南","originalKeyword":"湖南"}],"language":"zh","publisherId":"huangj201302005","title":"湖南省隆回县杏枫山金矿床地质特征及成矿模式探讨","volume":"34","year":"2013"},{"abstractinfo":"建立了基于液相色谱-离子阱飞行时间串联质谱(LC-IT-TOF MS/MS)的酚酸类分析方法,对6种共18批次的石斛枫斗药材中的酚类化合物进行了研究,其中18种酚酸类化合物得到初步定性.在共有化合物中选择杓唇石斛素和石斛酚作为质量控制的目标化合物.在此基础上,采用响应面法(RSM)确定了提取溶剂为60%甲醇、提取时间为65 min的超声提取杓唇石斛素和石斛酚的最佳条件,建立了石斛枫斗中杓唇石斛素、石斛酚的高效液相色谱(HPLC)含量测定方法.定量线性优于0.999 8,检出限(LOD)分别为0.18 mg/L 和0.09 mg/L,重复性的相对标准偏差(RSD)小于3% ,加标回收率均值分别为97.1%和101.4% .这些结果表明本研究建立的方法可用于石斛枫斗药材中酚酸类化学成分研究及质量控制.","authors":[{"authorName":"周婧","id":"067cb7e8-095c-40fc-8ecb-c08d377f8c8f","originalAuthorName":"周婧"},{"authorName":"许志良","id":"4b98e4e2-43ba-4491-90bd-b0229a9a86fe","originalAuthorName":"许志良"},{"authorName":"孔宏伟","id":"382243e4-e058-4a55-a253-789791aef19e","originalAuthorName":"孔宏伟"},{"authorName":"路鑫","id":"54ea0da4-e9a8-49cd-9f2f-2d6da90c5570","originalAuthorName":"路鑫"},{"authorName":"许国旺","id":"f00dafb0-cfdd-4af2-9106-9e1956277234","originalAuthorName":"许国旺"}],"doi":"10.3724/SP.J.1123.2010.00566","fpage":"566","id":"86c11be2-2c95-4665-a82b-8da6eaa9c95f","issue":"6","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"9cacd447-3042-4773-b8b5-edfa1d879917","keyword":"液相色谱-离子阱飞行时间串联质谱","originalKeyword":"液相色谱-离子阱飞行时间串联质谱"},{"id":"7e8da7a8-b7a1-4016-9785-09397dc229b3","keyword":"含量","originalKeyword":"含量"},{"id":"255b5145-2ae0-4496-b5e8-af6d7c36757b","keyword":"酚酸类物质","originalKeyword":"酚酸类物质"},{"id":"6b62b59f-8b15-47bb-b404-9f44f2ed1a21","keyword":"杓唇石斛素","originalKeyword":"杓唇石斛素"},{"id":"ce7e68d3-5e3d-438c-9be8-52d175dbc4b8","keyword":"石斛酚","originalKeyword":"石斛酚"},{"id":"77826760-45f4-4cd4-ae05-bc1e1ec9dfeb","keyword":"石斛枫斗","originalKeyword":"石斛枫斗"}],"language":"zh","publisherId":"sp201006009","title":"不同石斛枫斗中酚酸类活性成分的比较及杓唇石斛素和石斛酚含量的测定","volume":"28","year":"2010"},{"abstractinfo":"本文通过CaCl2·2H2O与药物奥沙拉秦及辅助配体邻菲罗啉在水热条件下得到了一个新的奥沙拉秦配合物[ Ca(L) (Phen)·4(H2O)]n(H2L=奥沙拉秦=3,3-azo-bis-6-hydroxybenzoic acid)(1).通过元素分析、红外对配合物进行了表征,并利用X单晶射线衍射仪测定了其结构.结构解析表明,配合物1属三斜晶系,空间群P-1,晶胞参数a=0.8001 (3) nm,b=1.1245(4) nm,c=1.5129(6) nm,α=89.450(6)°,β=86.297(6)°,γ=77.633(6)°,V=1.3268(9) nm3,Z=2,F(000) =636,最终偏差因子(对Ⅰ＞2σ(Ⅰ)的衍射点),R1=0.0521,wR2 =0.1538,S=1.045.在该结构中,中心Ca(Ⅱ)离子周围形成了一个稍微扭曲的五角双锥体,分别与一个来自奥沙拉秦配体的羧基氧原子(单齿)、两个邻菲罗啉中的两个N原子和四个水分子配位.","authors":[{"authorName":"唐云志","id":"4925f4dc-4c48-4843-a2cc-1db1d64d57f8","originalAuthorName":"唐云志"},{"authorName":"周漫","id":"61198b00-dfa9-4269-a0be-54b2b5545119","originalAuthorName":"周漫"},{"authorName":"杨燕明","id":"f563512e-b38d-43eb-b798-6888f00257bf","originalAuthorName":"杨燕明"},{"authorName":"王小卫","id":"ad42e292-1dcd-44c4-93a7-409bb8001891","originalAuthorName":"王小卫"},{"authorName":"黄帅","id":"b64f91a6-1355-4486-86e8-ee7f803a143f","originalAuthorName":"黄帅"}],"doi":"","fpage":"1083","id":"c596b76b-0fba-45b7-b4df-4b93ece4e257","issue":"4","journal":{"abbrevTitle":"RGJTXB","coverImgSrc":"journal/img/cover/RGJTXB.jpg","id":"57","issnPpub":"1000-985X","publisherId":"RGJTXB","title":"人工晶体学报"},"keywords":[{"id":"0a8b85fc-8ac3-4d26-b683-8dc716dfdafb","keyword":"奥沙拉秦","originalKeyword":"奥沙拉秦"},{"id":"1e431483-9972-427e-a9a8-4c924bf5bf77","keyword":"钙配合物","originalKeyword":"钙配合物"},{"id":"9387043d-4593-44ac-99b9-170ef63fd5cb","keyword":"晶体结构","originalKeyword":"晶体结构"}],"language":"zh","publisherId":"rgjtxb98201104051","title":"奥沙拉秦钙配合物的合成、结构及表征","volume":"40","year":"2011"},{"abstractinfo":"铸机拉矫机万向联轴器主要是将减速机扭矩传递给扇形段驱动辊,为连铸机提供拉矫力.首秦3号连铸机万向联轴器伸缩位置距离扇形段驱动辊连接法兰较近,在二冷室内极易腐蚀锈死,不易拆卸;同时万向联轴器与扇形段驱动辊法兰连接处螺栓极易松动,造成引锭杆下沉,严重影响生产.对拉矫机万向联轴进行技术改造,解决了万向联轴器伸缩腐蚀锈死和万向联轴器与扇形段驱动辊法兰盘螺栓容易松动的问题.","authors":[{"authorName":"樊星辰","id":"5ab6d982-69f1-4e21-92d8-ab946c50f200","originalAuthorName":"樊星辰"},{"authorName":"孙博","id":"cb232e5f-de67-421c-91df-a2569f0418db","originalAuthorName":"孙博"},{"authorName":"贾广顺","id":"c5d9522c-897c-425b-86df-4845a06f4544","originalAuthorName":"贾广顺"},{"authorName":"李松山","id":"7137d758-8426-4cb3-8946-3c4773c5ab85","originalAuthorName":"李松山"},{"authorName":"甄新刚","id":"a8a3ab03-2194-4740-a76e-1e5e857eb9c7","originalAuthorName":"甄新刚"}],"doi":"","fpage":"35","id":"19ead3c4-f51d-4b40-a812-60e9ff62355d","issue":"5","journal":{"abbrevTitle":"LZ","coverImgSrc":"journal/img/cover/LZ.jpg","id":"52","issnPpub":"1005-4006","publisherId":"LZ","title":"连铸"},"keywords":[{"id":"02c476bf-a9de-4210-a3e1-2182bb07e068","keyword":"万向联轴器","originalKeyword":"万向联轴器"},{"id":"25d9c5e4-7bcc-4ed0-8c46-9d25d37c2496","keyword":"法兰","originalKeyword":"法兰"},{"id":"18d80733-4335-4f27-be41-b10ca59fa787","keyword":"伸缩","originalKeyword":"伸缩"},{"id":"44172b07-a019-413c-aea6-581bd92291b7","keyword":"扭矩","originalKeyword":"扭矩"}],"language":"zh","publisherId":"lz201305008","title":"首秦3号板坯铸机拉矫机万向联轴器改造","volume":"","year":"2013"},{"abstractinfo":"首秦1号高炉的技术装备、工艺水平、自动控制和环保节能等方面的新技术都达到了较高水平。高炉达到设计指标后，在原燃料质量不断提高的同时，采用技术创新与技术进步，解决了高炉单系统流程给生产带来的新问题，使得新技术、新装备能力达到较高水平，生产综合指标不断提高。实现燃料比低于492 kg/t，煤比高于180kg/t，在国内同类高炉中位于领先的水平。","authors":[{"authorName":"丁汝才","id":"7c36ff97-fde2-4012-8d2e-07cc8d93c8c7","originalAuthorName":"丁汝才"},{"authorName":"吴铿","id":"656d3002-702a-435d-acac-cf692bc1b623","originalAuthorName":"吴铿"},{"authorName":"尹晓莹","id":"14844a2c-3b1e-46e1-86fb-f5ff0f002083","originalAuthorName":"尹晓莹"},{"authorName":"费三林","id":"e520f12e-322e-4b6c-ac7e-a3609af94eea","originalAuthorName":"费三林"},{"authorName":"何海熙","id":"7b809c48-a667-4617-98b7-b5ecfd84f141","originalAuthorName":"何海熙"},{"authorName":"韦少华","id":"1c537474-39e8-441c-ba2b-db8c0a5be52d","originalAuthorName":"韦少华"}],"categoryName":"|","doi":"","fpage":"18","id":"1ab220d5-e906-4a63-84b0-dd8d6f810be2","issue":"3","journal":{"abbrevTitle":"GT","coverImgSrc":"journal/img/cover/GT.jpg","id":"27","issnPpub":"0449-749X","publisherId":"GT","title":"钢铁"},"keywords":[{"id":"684dffb9-58b6-4546-b682-b161ef63ab53","keyword":"高炉;燃料比;喷煤比;高炉操作","originalKeyword":"高炉;燃料比;喷煤比;高炉操作"}],"language":"zh","publisherId":"0449-749X_2009_3_10","title":"首秦1号高炉降低燃料比和提高喷煤比的工业实践","volume":"44","year":"2009"},{"abstractinfo":"首秦1号高炉的技术装备、工艺水平、自动控制和环保节能等方面的新技术都达到了较高水平.高炉达到设计指标后,在原燃料质量不断提高的同时,采用技术创新与技术进步,解决了高炉单系统流程给生产带来的新问题,使得新技术、新装备能力达到较高水平,生产综合指标不断提高.实现燃料比低于492 kg/t,煤比高于180kg/t,在国内同类高炉中位于领先的水平.","authors":[{"authorName":"丁汝才","id":"04f8e80f-f7b2-4b61-a52d-f99f6d333691","originalAuthorName":"丁汝才"},{"authorName":"吴铿","id":"847b5a38-99df-4a4f-b5ad-fc2a21304b88","originalAuthorName":"吴铿"},{"authorName":"尹晓莹","id":"f6db2c89-76ab-42ef-a508-3e9c94245bdc","originalAuthorName":"尹晓莹"},{"authorName":"费三林","id":"d10abfae-a20c-4d02-87ba-ed77254648e9","originalAuthorName":"费三林"},{"authorName":"何海熙","id":"be35429c-a23c-48f2-a6d4-3ee482f1db01","originalAuthorName":"何海熙"},{"authorName":"韦少华","id":"d492e394-dc83-458d-8528-dcd2ad4bb6ba","originalAuthorName":"韦少华"}],"doi":"","fpage":"18","id":"36f4c72c-b0d6-4125-a4ca-d11ed81f6ebc","issue":"3","journal":{"abbrevTitle":"GT","coverImgSrc":"journal/img/cover/GT.jpg","id":"27","issnPpub":"0449-749X","publisherId":"GT","title":"钢铁"},"keywords":[{"id":"e70edb1d-9103-4c83-ad5c-29acb04f1a12","keyword":"高炉","originalKeyword":"高炉"},{"id":"9cc98ff2-2c37-4b0d-aef4-83428d548ab8","keyword":"燃料比","originalKeyword":"燃料比"},{"id":"50e31976-85fc-4ab7-822f-9223ea625953","keyword":"喷煤比","originalKeyword":"喷煤比"},{"id":"6881b5d2-02da-4337-a511-0432bdcbccff","keyword":"高炉操作","originalKeyword":"高炉操作"}],"language":"zh","publisherId":"gt200903005","title":"首秦1号高炉降低燃料比和提高喷煤比的工业实践","volume":"44","year":"2009"},{"abstractinfo":"以首秦4 300 mm宽厚板生产线为例,介绍高压水除磷系统的设计方案,对供水能力进行计算,同时针对在实际生产过程中存在的问题,提出可行的改造方案,给出改造后除磷泵设备的工艺参数及各用水点的压力和流量,最后进行提高系统压力后供水能力核算,验证改造方案的可行性.结果表明,在不改变系统电机容量的前提下,通过改进喷嘴结构和增加除鳞泵的级数可以提高系统的压力,并进一步优化除磷效果.","authors":[{"authorName":"孟祥龙","id":"5b5720bd-981e-4996-9d03-fa124ef0fb53","originalAuthorName":"孟祥龙"},{"authorName":"侯宏宙","id":"6f3aef72-cec4-444f-bf1f-6a828214c739","originalAuthorName":"侯宏宙"},{"authorName":"李林","id":"631d69aa-cc52-44dd-ae95-8412da0ca790","originalAuthorName":"李林"},{"authorName":"王帆","id":"02f6fa80-6279-40f4-97f8-330f7017c978","originalAuthorName":"王帆"},{"authorName":"王向阳","id":"0b5b6dc1-2e3c-4f9e-96cb-6b66d5050064","originalAuthorName":"王向阳"}],"doi":"","fpage":"49","id":"d0c7143e-1626-43e1-9b80-43409bbcd86e","issue":"2","journal":{"abbrevTitle":"SHJS","coverImgSrc":"journal/img/cover/SHJS.jpg","id":"59","issnPpub":"1001-7208","publisherId":"SHJS","title":"上海金属"},"keywords":[{"id":"3b063a0d-38bc-4136-a72c-8a3e5cc9a38a","keyword":"轧钢","originalKeyword":"轧钢"},{"id":"88338cdf-6980-4ae6-92a7-fc64a9f3fb74","keyword":"宽厚板","originalKeyword":"宽厚板"},{"id":"2afcf8c0-e257-447c-9605-43a661e9e8b6","keyword":"高压水","originalKeyword":"高压水"},{"id":"c37746d3-12da-46fd-a365-a5e0e5ee2aed","keyword":"除磷","originalKeyword":"除磷"}],"language":"zh","publisherId":"shjs201502012","title":"首秦宽厚板生产线高压水除鳞系统设计及改造","volume":"37","year":"2015"},{"abstractinfo":"采用顶空气相色谱法对秦龙苦素中残留的苯、甲苯、对二甲苯、正己烷等有害物质进行分析,并讨论了流速、柱温、平衡温度、平衡时间、抽样次数等因素对测定的影响.分析结果表明,该方法对上述4种有害物质的检测限范围为3～98 μg/L,测定结果的相对标准偏差为0.59%～2.64%,样品的回收率为97.2%～120.0%.方法简便、快速、灵敏、重现性好.","authors":[{"authorName":"汤桦","id":"bb5c8dba-d316-4058-8144-93de18d78dae","originalAuthorName":"汤桦"},{"authorName":"雷根虎","id":"37a5f260-cb18-4f4f-ae7f-0dede36445db","originalAuthorName":"雷根虎"},{"authorName":"李鹏","id":"df3c18f8-910e-4e68-b1c7-dfe1b0afdce4","originalAuthorName":"李鹏"},{"authorName":"孔祥虹","id":"c2182739-8f21-4572-a347-91083316d0b9","originalAuthorName":"孔祥虹"},{"authorName":"何学文","id":"e4e43388-8536-4bba-8357-2407220317c1","originalAuthorName":"何学文"}],"doi":"10.3321/j.issn:1000-8713.2003.02.021","fpage":"178","id":"c1629525-b3df-492d-b576-498623d83cd2","issue":"2","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"9d62659d-e61f-4362-a788-69fc69402d44","keyword":"顶空气相色谱法","originalKeyword":"顶空气相色谱法"},{"id":"03a44d3b-a3e0-4d92-ad83-ee6c022e5fa8","keyword":"秦龙苦素","originalKeyword":"秦龙苦素"},{"id":"30e1d312-6b9a-4df2-9dd6-77abaf78c21c","keyword":"溶剂残留","originalKeyword":"溶剂残留"}],"language":"zh","publisherId":"sp200302021","title":"顶空气相色谱法测定秦龙苦素中的残留溶剂","volume":"21","year":"2003"},{"abstractinfo":"捣固焦由于成本低且性能指标较好而逐步推广使用，然而首秦高炉在使用捣固焦后出现了炉内压量关系紧张、炉况不顺等问题。为了了解这批焦炭的实际性能，进行了反应性试验、差热试验以及光学组织含量分析，结果表明：焦炭光学组织中镶嵌结构有抑制裂纹发展和缓解热膨胀的作用，而捣固焦的镶嵌组织含量较低，因此在高温和冲击受力的作用下更容易产生裂纹；分析6种焦粉失重曲线可以发现，同性组分ΣISO含量高的捣固焦粉从1000升高到1300℃过程中汽化反应失重率增加更快，在炉内可能引起的粒度降解更严重，从而造成炉况不顺。","authors":[{"authorName":"马超","id":"ba6c97d3-35d2-4837-b3c1-76a2140a266f","originalAuthorName":"马超"},{"authorName":"晁伟","id":"73b269cf-757c-4b0c-bec6-65d0868d4cd7","originalAuthorName":"晁伟"},{"authorName":"李东涛","id":"051ee634-2ce6-4eed-80d2-727cde5af66e","originalAuthorName":"李东涛"},{"authorName":"刘洋","id":"fc3e2bf1-f036-4b58-99d6-2e34c2a8a2fd","originalAuthorName":"刘洋"},{"authorName":"徐萌","id":"fdadd0fc-c2d1-4837-9002-0dbb6f59dd98","originalAuthorName":"徐萌"},{"authorName":"徐荣广","id":"0b8c6729-c888-4c71-a87b-29b4d87c45a8","originalAuthorName":"徐荣广"}],"doi":"10.13228/j.boyuan.issn0449-749x.20130692","fpage":"33","id":"cf4f3534-c822-4a0d-b820-0d450ced9335","issue":"12","journal":{"abbrevTitle":"GT","coverImgSrc":"journal/img/cover/GT.jpg","id":"27","issnPpub":"0449-749X","publisherId":"GT","title":"钢铁"},"keywords":[{"id":"fb9f6f41-8d9c-45c9-b5df-569a822dec67","keyword":"焦炭","originalKeyword":"焦炭"},{"id":"01cf423d-aa39-454b-a20c-151d66dbb0d2","keyword":"捣固焦","originalKeyword":"捣固焦"},{"id":"5d28cd23-9cb0-4f6d-a70c-4b51c110fb4a","keyword":"汽化反应","originalKeyword":"汽化反应"},{"id":"acae6b69-df6f-433e-8e10-723327cd9390","keyword":"光学组织","originalKeyword":"光学组织"},{"id":"a707a203-f658-413f-962e-fa635a680970","keyword":"气孔","originalKeyword":"气孔"}],"language":"zh","publisherId":"gt201412007","title":"首秦焦炭碳素溶蚀能力与显微结构的相关性","volume":"","year":"2014"}],"totalpage":291,"totalrecord":2904}