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style=\"color:red\">鹏</span>","id":"770a61de-ee52-4c13-9f4a-c76a7dab39f5","originalAuthorName":"卓鹏"},{"authorName":"陈志平","id":"e2600364-8eb7-4235-a87f-29db9791826a","originalAuthorName":"陈志平"},{"authorName":"丛晶洁","id":"1f91ff6a-75a3-43b2-a186-e646f2ce74f6","originalAuthorName":"丛晶洁"},{"authorName":"张璇","id":"52def255-6925-4f7a-9695-6fbb546c8dc6","originalAuthorName":"张璇"}],"doi":"","fpage":"1046","id":"d26c0151-7063-4474-88da-8f6c3822beb3","issue":"4","journal":{"abbrevTitle":"FHCLXB","coverImgSrc":"journal/img/cover/FHCLXB.jpg","id":"26","issnPpub":"1000-3851","publisherId":"FHCLXB","title":"复合材料学报"},"keywords":[{"id":"5c65e25d-d4f5-49f0-b230-61ea06567c5f","keyword":"VARI","originalKeyword":"VARI"},{"id":"aae3540f-957a-4026-8a93-57d878943aa3","keyword":"真空渗漏","originalKeyword":"真空渗漏"},{"id":"a5df7719-f714-4a4d-8163-3038f79cbcf0","keyword":"成型质量","originalKeyword":"成型质量"},{"id":"149a1ced-2972-4d9c-bdf9-343681b1a0ea","keyword":"复合材料","originalKeyword":"复合材料"},{"id":"f1c35fbd-eb9b-44f7-b266-41934740a22f","keyword":"开孔压缩性能","originalKeyword":"开孔压缩性能"}],"language":"zh","publisherId":"fhclxb201404026","title":"真空渗漏工艺缺陷对VARI成型复合材料质量及性能的影响","volume":"31","year":"2014"},{"abstractinfo":"<span style=\"color:red\">卓</span>家庄金矿床是一个与中生代次火山杂岩体(二长闪长玢岩、二长斑岩)有关的小型金矿床,柱状矿体严格地受隐爆角砾岩筒的控制.从角砾岩筒中心向外,角砾粒度、成分、胶结物成分及蚀变均存在分带现象.全文着重阐述了金矿床地质特征,总结出矿床成矿规律,并对矿区成矿远景作了预测.","authors":[{"authorName":"祝德平","id":"b64c2825-d8a8-4a16-bfca-1523ba46f91b","originalAuthorName":"祝德平"},{"authorName":"于超","id":"efdb554f-3afa-445b-a7cd-d2dfaf10e18f","originalAuthorName":"于超"},{"authorName":"廉永","id":"0da023aa-5664-4296-b261-9119c90abb01","originalAuthorName":"廉永"},{"authorName":"杨忠臣","id":"e60999c8-666f-4d0d-98c4-e37f37dc2434","originalAuthorName":"杨忠臣"},{"authorName":"齐可昆","id":"f2d84302-f718-47b9-9f01-a71c519c2e97","originalAuthorName":"齐可昆"}],"doi":"10.3969/j.issn.1001-1277.2001.08.003","fpage":"11","id":"cbd7cad8-5e0a-46fc-acf8-3878f17bd5b5","issue":"8","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"851dbe8d-889e-41e9-8802-2225d6c86a5b","keyword":"次火山杂岩体","originalKeyword":"次火山杂岩体"},{"id":"37060356-312b-4ecd-96eb-216032b31ecc","keyword":"角砾岩筒型金矿床","originalKeyword":"角砾岩筒型金矿床"},{"id":"c7d6e2a9-6cbe-4a48-b458-c595a122c4a2","keyword":"地质特征","originalKeyword":"地质特征"},{"id":"58249dda-b9dc-4a14-8037-fce33acb21b0","keyword":"成矿规律","originalKeyword":"成矿规律"},{"id":"8ae8b516-06c4-4a87-8083-fdd24e15866e","keyword":"<span style=\"color:red\">卓</span>家庄","originalKeyword":"卓家庄"}],"language":"zh","publisherId":"huangj200108003","title":"平邑<span style=\"color:red\">卓</span>家庄金矿床成矿地质特征","volume":"22","year":"2001"},{"abstractinfo":"按Koenigs-Knorr 方法将四乙酰溴代半乳糖分别与3-乙酰基<span style=\"color:red\">卓</span>酚酮和3-乙酰胺基<span style=\"color:red\">卓</span>酚酮以Ag2CO3为催化剂反应合成了β-构型糖苷. 由于<span style=\"color:red\">卓</span>酚酮存在互变异构,糖基化物亦为2种异构产物. 应用元素分析、核磁共振、红外光谱表征了它们的结构. 分析结果表明,所得到的化合物是含有<span style=\"color:red\">卓</span>酚酮基团的四乙酰基β-构型半乳糖苷.","authors":[{"authorName":"钟方丽","id":"5bcf4273-a895-4e07-a8de-1da49efa90c5","originalAuthorName":"钟方丽"},{"authorName":"王晓林","id":"427d3a85-6d9c-432d-ab58-3b47fd8b1130","originalAuthorName":"王晓林"},{"authorName":"尹丙柱","id":"71e6bcda-a262-4726-8dfa-1968f8a88d7d","originalAuthorName":"尹丙柱"},{"authorName":"金钟天","id":"9fd0dacc-c138-45a9-b7c4-06063ecd1f3e","originalAuthorName":"金钟天"}],"doi":"10.3969/j.issn.1000-0518.2004.05.016","fpage":"502","id":"59317e1b-b244-4733-8df4-413a60833734","issue":"5","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"fc2d1bb3-7de4-4c97-b819-0d43a58278e3","keyword":"环庚三烯酚酮","originalKeyword":"环庚三烯酚酮"},{"id":"66daf074-3e44-4c48-b0e8-7f0252d50ef7","keyword":"半乳糖苷","originalKeyword":"半乳糖苷"},{"id":"67587e24-3aec-4a3e-af0f-675cd8894c78","keyword":"Koenigs-Knorr糖基化反应","originalKeyword":"Koenigs-Knorr糖基化反应"}],"language":"zh","publisherId":"yyhx200405016","title":"含<span style=\"color:red\">卓</span>酚酮基团的四乙酰基半乳糖苷的合成","volume":"21","year":"2004"},{"abstractinfo":"西藏隆子县邦<span style=\"color:red\">卓</span>玛金矿床是近年通过区域地质调查新发现的金矿床.重点对邦<span style=\"color:red\">卓</span>玛金矿床的矿床地质特征及地球化学异常特征进行了系统总结,以期为今后的勘探工作提供基础资料及依据.矿体主要产于上三叠统涅如组二段中,受东西向次级断裂构造带控制;目前共发现金矿脉9条,圈定5个金矿体.通过开展土壤地球化学剖面测量工作,选择了Au、Sb、Pb、Zn、Sn、As作为Au及多金属成矿指示元素,共圈定单元素异常40处,圈定组合异常5处,各组合异常内元素套合较好.综合分析认为,区内找矿前景较大,具有进一步工作价值.","authors":[{"authorName":"陈东太","id":"31c82be1-3050-4004-95ee-659b0ad8962b","originalAuthorName":"陈东太"},{"authorName":"陈武","id":"9a5ad4e7-a819-442c-8007-3f0808a3facb","originalAuthorName":"陈武"},{"authorName":"胡可卫","id":"b3a773ee-76c2-4ca1-9c92-2cddcc9be689","originalAuthorName":"胡可卫"},{"authorName":"余杰","id":"a2ca40f9-0197-408d-bd5f-1de9ba133340","originalAuthorName":"余杰"},{"authorName":"黄青东智","id":"17d2088a-35e1-4f7e-82d1-dd1a35a2fc11","originalAuthorName":"黄青东智"}],"doi":"10.11792/hj20160806","fpage":"25","id":"07ef87d3-c8b7-4ecc-b284-b8e226b06895","issue":"8","journal":{"abbrevTitle":"HJ","coverImgSrc":"journal/img/cover/HJ.jpg","id":"44","issnPpub":"1001-1277","publisherId":"HJ","title":"黄金"},"keywords":[{"id":"8b69150b-2bdc-4dac-b766-51f3a6a1ac60","keyword":"地质特征","originalKeyword":"地质特征"},{"id":"89b57898-7f81-4529-b043-3665884e940f","keyword":"地球化学异常特征","originalKeyword":"地球化学异常特征"},{"id":"ca84ca9a-7896-4be0-92ef-013b77707b64","keyword":"邦<span style=\"color:red\">卓</span>玛金矿床","originalKeyword":"邦卓玛金矿床"}],"language":"zh","publisherId":"huangj201608006","title":"西藏隆子县邦<span style=\"color:red\">卓</span>玛金矿床地质特征及地球化学异常特征","volume":"37","year":"2016"},{"abstractinfo":"采用 C18反相色谱柱，以磺丁基醚-β-环糊精（SBE-β-CD）作为手性流动相添加剂，建立了阿<span style=\"color:red\">卓</span>乳酸对映体的高效液相色谱拆分方法。考察了环糊精衍生物类型、手性添加剂浓度、流动相 pH、流速和柱温对手性分离的影响，同时探讨了高效液相色谱采用磺丁基醚-β-环糊精分离阿<span style=\"color:red\">卓</span>乳酸对映体的分离机制及包结常数，确定了色谱条件为YMC-Pack ODS-A C18色谱柱（250 mm×4.6 mm，5μm），流动相为含25 mmol / L SBE-β-CD 的0.1 mol / L 磷酸盐缓冲液（pH 2.68）-乙腈（90∶10，v / v），流速为0.6 mL / min，柱温为30℃，紫外检测波长为220 nm。对映体的保留时间分别为26.65和28.28 min，分离度为1.68。本方法分离度好，简便易行，且比使用手性固定相分离更加经济。","authors":[{"authorName":"张虎","id":"199ed0ce-33f6-4cf1-bf40-c7b864809daf","originalAuthorName":"张虎"},{"authorName":"沈芒芒","id":"1278c4b9-ee74-48cd-8c74-a499e47ae642","originalAuthorName":"沈芒芒"},{"authorName":"童胜强","id":"74a82a16-3008-43cc-8531-172a7ea97a0c","originalAuthorName":"童胜强"},{"authorName":"颜继忠","id":"18bbb8dd-ce09-4974-8de8-7bb091a54fd6","originalAuthorName":"颜继忠"}],"doi":"10.3724/SP.J.1123.2014.02023","fpage":"612","id":"97d75d10-0262-4e2c-a4d4-7696aedf14ea","issue":"6","journal":{"abbrevTitle":"SP","coverImgSrc":"journal/img/cover/SP.jpg","id":"58","issnPpub":"1000-8713","publisherId":"SP","title":"色谱 "},"keywords":[{"id":"d5612498-ee90-4c5a-b07d-4b8f15a7972c","keyword":"高效液相色谱","originalKeyword":"高效液相色谱"},{"id":"156c40b2-3630-4c61-adf9-551ad77b2f23","keyword":"手性流动相添加法","originalKeyword":"手性流动相添加法"},{"id":"076dc4a7-c05b-4b52-a0f9-1fddb6230bbb","keyword":"阿<span style=\"color:red\">卓</span>乳酸","originalKeyword":"阿卓乳酸"},{"id":"e3775a48-af0e-4030-8582-84b14aacdeb4","keyword":"对映体拆分","originalKeyword":"对映体拆分"},{"id":"a29d38c2-ad60-4dc5-9db2-6b6087e5bcd6","keyword":"磺丁基醚-β-环糊精","originalKeyword":"磺丁基醚-β-环糊精"}],"language":"zh","publisherId":"sp201406009","title":"高效液相色谱手性流动相添加法拆分阿<span style=\"color:red\">卓</span>乳酸对映体","volume":"","year":"2014"},{"abstractinfo":"以2-甲硫基苯胺为原料,通过酰化、碘环化以及Suzuki交叉偶联反应,合成了5-甲基-2,3-二苯基-1,5-苯并硫氮杂<span style=\"color:red\">卓</span>-4(5H)-酮.分别考察了催化剂对酰化反应、溶剂对碘环化反应的影响,以及催化剂、配体、碱和温度等因素对Suzuki交叉偶联反应的影响,在最佳的反应条件下,反应总收率为68.5%,中间产物和目标产物的结构经IR、NMR和MS等测试技术得以确证.","authors":[{"authorName":"陶李明","id":"fe01102b-d9c4-4044-b342-dcfccf3c680d","originalAuthorName":"陶李明"},{"authorName":"刘文奇","id":"d26498e5-0edc-4be8-b928-27e99afdbd3e","originalAuthorName":"刘文奇"},{"authorName":"谭倪","id":"8b442191-5716-4c12-80b4-0e75d6b16fe9","originalAuthorName":"谭倪"},{"authorName":"周芸","id":"f41109e3-dab5-40cc-9102-618bec540570","originalAuthorName":"周芸"}],"doi":"10.3724/SP.J.1095.2010.90420","fpage":"494","id":"7092b62d-fb07-413f-8383-3d0331af024b","issue":"4","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"2d8e3617-a317-4233-9046-5dd00ddbc88f","keyword":"甲基二苯基苯并硫氮杂<span style=\"color:red\">卓</span>-4(5H)-酮","originalKeyword":"甲基二苯基苯并硫氮杂卓-4(5H)-酮"},{"id":"78749312-e1d2-4593-a68a-eff0cfff001c","keyword":"酰化反应","originalKeyword":"酰化反应"},{"id":"d3930d7c-93fe-466c-8e40-9127e1e8065e","keyword":"碘环化反应","originalKeyword":"碘环化反应"},{"id":"a1e63284-2324-49be-b7d4-7768e38ae1ab","keyword":"Suzuki交叉偶联反应","originalKeyword":"Suzuki交叉偶联反应"}],"language":"zh","publisherId":"yyhx201004027","title":"5-甲基-2,3-二苯基-1,5-苯并硫氮杂<span style=\"color:red\">卓</span>-4(5H)-酮的合成","volume":"27","year":"2010"},{"abstractinfo":"将1,2,3-三唑环结构及1,2,4-噁二唑环等多个药效团结构叠加到同一个硫氮杂<span style=\"color:red\">卓</span>分子中,为药理及生理活性研究提供较好的先导化合物.反应在三乙胺存在下,用2,4-二芳基-2,3-二氢-1,5-苯并硫氮杂<span style=\"color:red\">卓</span>与α-氯代-2-苯基-1,2,3-三唑基-4-甲醛肟在室温进行1,3-偶极环加成反应,合成一系列的2-苯基-1,2,3-三唑基[1,2,4]噁二唑并[4,5-a][1,5]苯并硫氮杂<span style=\"color:red\">卓</span>化合物,并采用红外光谱、核磁共振、元素分析等测试技术对化合物进行了表征.","authors":[{"authorName":"王冉冉","id":"d1679f9a-d00c-426f-b761-fe1c32a74868","originalAuthorName":"王冉冉"},{"authorName":"梁平","id":"87b55903-9ced-491b-acbd-6f8aae54ab4c","originalAuthorName":"梁平"},{"authorName":"解正峰","id":"25675b0b-de7b-4851-ba71-06db1766642d","originalAuthorName":"解正峰"},{"authorName":"刘方明","id":"c9c40af9-d35f-422d-8802-bafa55a31f33","originalAuthorName":"刘方明"}],"doi":"10.3969/j.issn.1000-0518.2008.12.003","fpage":"1389","id":"304d95a6-d371-4e3b-b047-320bdc0df3ea","issue":"12","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"2bc103f9-0c67-41f9-b50f-c0d5a3e5171a","keyword":"环加成反应","originalKeyword":"环加成反应"},{"id":"ee990ec5-9600-4dbf-8d89-cacfbb4b9749","keyword":"肟","originalKeyword":"肟"},{"id":"af620d03-fb44-4244-aa2d-98bffe2db7f8","keyword":"苯并硫氮杂<span style=\"color:red\">卓</span>","originalKeyword":"苯并硫氮杂卓"},{"id":"34f9c5e6-d989-48b2-9783-c41005ebc31b","keyword":"合成","originalKeyword":"合成"}],"language":"zh","publisherId":"yyhx200812003","title":"新型含1,2,3-三唑基[1,2,4](噁)二唑并[4,5-a][1,5]苯并硫氮杂<span style=\"color:red\">卓</span>化合物的合成","volume":"25","year":"2008"},{"abstractinfo":"以对甲苯磺酰氯和邻氨基苯甲酸甲酯为原料,通过酰胺化、酰亚胺和卤代烃的缩合、克曼环化及水解脱羧等反应,合成盐酸考尼伐坦关键中间体N-甲苯磺酰基苯并氮杂<span style=\"color:red\">卓</span>-5-酮.在合成过程中,分别减少了有毒溶剂吡啶的用量,用叔丁醇钾代替怕水易爆的氢化钠,用容易购买回收的2-甲基四氢呋喃代替丁酮为溶剂,目标化合物的总收率由55％提高至63％,纯度达到99％以上.所得化合物经熔点、核磁共振氢谱等得到确认.该工艺显著地提高了中间体的产量及质量,因而提高了盐酸考尼伐坦的产率.","authors":[{"authorName":"马亚娟","id":"5387b4c3-9c87-4fbc-8c17-8903c62597d0","originalAuthorName":"马亚娟"},{"authorName":"李晓东","id":"bbb50240-fc8a-4523-bed2-e0c10fe2cb0c","originalAuthorName":"李晓东"},{"authorName":"李蕴","id":"88a9f80a-1643-4711-babe-16dd21b12603","originalAuthorName":"李蕴"},{"authorName":"洪波","id":"e92379f9-8cbf-456b-8c71-4b5a18b764de","originalAuthorName":"洪波"},{"authorName":"周米平","id":"e2753906-85f8-49af-b32f-f01d08b55adf","originalAuthorName":"周米平"}],"doi":"10.3724/SP.J.1095.2014.30007","fpage":"50","id":"5e03996f-c95e-4ae3-8e43-71ec9eeafea3","issue":"1","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"c7e97e64-6ec2-4157-8627-48204b309957","keyword":"盐酸考尼伐坦中间体","originalKeyword":"盐酸考尼伐坦中间体"},{"id":"668c5af9-aa45-4cf3-a2f4-e477c7b5214f","keyword":"N-甲苯磺酰基苯并氮杂<span style=\"color:red\">卓</span>酮","originalKeyword":"N-甲苯磺酰基苯并氮杂卓酮"},{"id":"60308630-4e4a-4332-9fed-49a779ce0dc2","keyword":"合成改进","originalKeyword":"合成改进"}],"language":"zh","publisherId":"yyhx201401008","title":"盐酸考尼伐坦关键中间体N-甲苯磺酰基苯并氮杂<span style=\"color:red\">卓</span>-5-酮合成工艺的改进","volume":"31","year":"2014"},{"abstractinfo":"用脯氨酸作为催化剂,研究了各种取代的二苯并1,4-氧氮杂<span style=\"color:red\">卓</span>衍生物类七元环状亚胺和丙酮的直接Mannich反应,该反应能高对映选择得到一系列旋光活性的含有β羰基的七元环状氮杂环化合物(93%–98%ee)。用丁酮作为Mannich给体时,能得到专一的区域选择性和96%–97%ee的产物。进一步通过X射线单晶衍射分析其中一个产物的衍生物,确定了产物手性中心绝对构型为R,其它同类型产物绝对构型随后通过化学类比方法推断确认。","authors":[{"authorName":"汪游清","id":"e6320dc5-b80e-4478-9c7c-4b9d1ef44586","originalAuthorName":"汪游清"},{"authorName":"任圆圆","id":"f9dc45d7-d834-4963-9d23-de7d6aa69de2","originalAuthorName":"任圆圆"}],"doi":"10.1016/S1872-2067(14)60225-4","fpage":"93","id":"15976e35-f440-40d4-b841-92a1b3a5f304","issue":"1","journal":{"abbrevTitle":"CHXB","coverImgSrc":"journal/img/cover/CHXB.jpg","id":"18","issnPpub":"0253-9837","publisherId":"CHXB","title":"催化学报   "},"keywords":[{"id":"4ccc934d-bfce-48c9-9187-7228017cd6e3","keyword":"丙酮","originalKeyword":"丙酮"},{"id":"d6cb7c83-e2b5-4f80-adea-20495c6bc739","keyword":"不对称催化","originalKeyword":"不对称催化"},{"id":"f690ea1b-851c-4152-af78-ab64479f67f6","keyword":"七元环状亚胺","originalKeyword":"七元环状亚胺"},{"id":"79fa8190-9f13-48fc-9bf4-76bc0697233e","keyword":"Mannich反应","originalKeyword":"Mannich反应"},{"id":"71fd8c48-299b-4859-8cad-3b0c7b9c7e9e","keyword":"有机催化","originalKeyword":"有机催化"}],"language":"zh","publisherId":"cuihuaxb201501016","title":"高对映选择性有机催化的七元环状亚胺二苯并1,4-氧氮杂<span style=\"color:red\">卓</span>和丙酮的直接Mannich反应","volume":"","year":"2015"},{"abstractinfo":"","authors":[],"doi":"","fpage":"72","id":"8f28ec39-605b-4b93-aab7-3c32e16e89bc","issue":"3","journal":{"abbrevTitle":"GSYTB","coverImgSrc":"journal/img/cover/GSYTB.jpg","id":"36","issnPpub":"1001-1625","publisherId":"GSYTB","title":"硅酸盐通报   "},"keywords":[{"id":"66819ad2-a6e4-48df-a815-71554b4ed50a","keyword":"","originalKeyword":""}],"language":"zh","publisherId":"gsytb200103017","title":"戴志良、杨自<span style=\"color:red\">鹏</span>同志被增补为中国硅酸盐学会第六届常务理事会常务理事","volume":"20","year":"2001"}],"totalpage":2,"totalrecord":18}