利用AEO7(脂肪醇聚氧乙烯(7)醚)/环己烷/正丁醇体系,以微乳液法制备超细钴黑陶瓷颜料.绘制了不同温度下AEO7/环己烷/正丁醇/水的拟三元相图；运用马尔文粒度分布仪测定了不同前驱离子浓度制备的钴黑颜料粒径；通过XRD和FT-IR测定了钴黑颜料物相及结构,采用UV-Vis和色差仪对钴黑颜料呈色进行分析.结果表明,该微乳液体系制备的钴黑颜料颗粒度随着前驱离子浓度降低而减小,粒度分布窄且均匀；钴黑颜料是系列尖晶石型物质；随着煅烧温度升高,钴黑颜料呈现较纯正黑色,偏红现象降低.
参考文献
| [1] | 张昭瑞,纪箴,王燕斌.溶胶-凝胶法制备MgO-Al2O3-SiO2系LTCC基板材料及其结构性能研究[J].功能材料,2008(01):72-74,78. |
| [2] | Zayat M.;Levy D. .Blue CoAl2O4 particles prepared by the sol-gel and citrate-gel methods[J].Chemistry of Materials,2000(9):2763-2769. |
| [3] | Felora Heshmatpour;Reza Babadi Aghakhanpour .Synthesis and characterization of nanocrystalline zirconia powder by simple sol-gel method with glucose and fructose as organic additives[J].Powder Technology: An International Journal on the Science and Technology of Wet and Dry Particulate Systems,2011(1/3):193-200. |
| [4] | 俞康泰,解茂林.化学共沉淀结合成Pr-.Nd-Zircon色料的研究[J].中国陶瓷,2000(05):1-3,14. |
| [5] | Zhizhan Chen;Erwei Shi;Wenjun Li .Hydrothermal synthesis and optical property of nano-sized CoAl_2O_4 pigment[J].Materials Letters,2002(5):281-284. |
| [6] | 姚朋军,王兢,赵林,戚金清,苏梅英.水热合成法制备La_（0.7）Sr_（0.3）FeO_3纳米线的合成机理研究[J].功能材料,2012(08):969-972. |
| [7] | Garcia A;Llusar M;Sorli S et al.Effect of the surfactant and precipitant on the synthesis of pink coral by a microemulsion method[J].Journal of the European Ceramic Society,2003,23(11):1829-1838. |
| [8] | Chen Jing;Shi Xiaobo Hanbing .The preparation and characteristics of cobalt blue colored mica titania pearlescent pigment by microemulsions[J].Dyes and Pigments,2007(3):766-769. |
| [9] | Zhu Zhenfeng;Wang Ruolan .Research progress on ceramic powder preqred by self-propagating high-temperating synthesis(SHS[J].china ceramics,2004,40(01):28-31. |
| [10] | 郭瑞松,赵丹,齐海涛.反相微乳液法非水相ZrO2陶瓷墨水的制备与性能[J].天津大学学报,2004(05):428-433. |
| [11] | Guo Ruisong;Qi Haitao;Chen Xianli et al.Prepapation of high concentration ZrO2 ceramic ink for jet-printing forming(Ⅰ[J].Journal of the Chinese Ceramic Society,2002,30(04):521-523. |
| [12] | 江红涛,王秀峰.反相微乳液法制备陶瓷彩喷墨水（Ⅰ）[J].中国陶瓷,2006(08):24-27. |
| [13] | 闻辂.矿物红外光谱学[M].重庆:重庆大学出版社,1989:115-116. |
| [14] | 廖立兵;王丽娟;尹京武.矿物材料现代测试技术[M].北京:化学工业出版社,2010:170-171. |
| [15] | S.A. Hosseini;A. Niaei;D. Salari .Nanocrystalline AMn_2O_4 (A = Co, Ni, Cu) spinels for remediation of volatile organic compounds-synthesis, characterization and catalytic performance[J].CERAMICS INTERNATIONAL,2012(2):1655-1661. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分：
-
10%
-
20%
-
30%
-
40%
-
50%