采用电沉积法在低碳钢基体上制备了韧性较好的镍镀层,并对镀镍钢带进行了拉伸试验.通过扫描电镜(SEM)和X射线衍射(XRD)分别对镍镀层变形前后的表面形貌和织构进行了研究.用纳米压痕的方法对拉伸变形前后的镍镀层样品进行了载荷-深度曲线的测试,并测量了电沉积镍镀层变形前后的硬度与杨氏模量.结果表明,拉伸变形后的镍镀层表面粗糙度变大,出现起皱,但并没有产生新的织构,只是原有织构的强度发生了变化,其硬度和杨氏模量都明显减小.对于同一样品,加不同载荷会导致不同的压痕深度,随深度的增加,测得的压痕硬度和样式模量也有明显降低.
参考文献
[1] | Tjong SC;Chen H .Nanocrystalline materials and coatings[J].Materials Science & Engineering, R. Reports: A Review Journal,2004(1/2):1-88. |
[2] | 黄勇力,章莎,赵冠湘,周益春,蒋艳平.用纳米压痕法测量电沉积镍镀层的应力-应变关系[J].湘潭大学自然科学学报,2006(02):47-51. |
[3] | Amit Kumar Gupta;D. Ravi Kumar .Formability of galvanized interstitial-free steel sheets[J].Journal of Materials Processing Technology,2006(2):225-237. |
[4] | L.Q. Zhou;Y.P. Li;Y.C. Zhou .Forming Limit of Electrodeposited Nickel Coating in the Left Region[J].Journal of Materials Engineering and Performance,2006(3):287-294. |
[5] | J. M. Lee;D. C. Ko;K. S. Lee;B. M. Kim .Identification of the bulk behavior of coatings by nano-indentation test and FE-analysis and its application to forming analysis of the coated steel sheet[J].Journal of Materials Processing Technology,2007(0):309-313. |
[6] | 辜敏,杨防祖,黄令,姚士冰,周绍民.高择优取向Cu电沉积层的XRD研究[J].电化学,2002(03):282-287. |
[7] | 孙增君 .选择合适的镀镍液处理方法[J].电镀与涂饰,1995,14(04):51-52. |
[8] | Chen JS.;Duh JG. .Indentation behavior and Young's modulus evaluation in electroless Ni modified CrN coating on mild steel[J].Surface & Coatings Technology,2001(1):6-13. |
[9] | S.Suresh;A.E.Glannakopoulos .A new method for estimating residual stresses by instrumented sharp indentation[J].Acta materialia,1998(16):5755-5768. |
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