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放电等离子烧结TiB2过程中真空室气压Pa有二个峰值,本文对Pa第二峰进行了研究.研究结果表明:Pa第二峰是烧结过程中化学反应导致的气相沉积所致.原始粉末和烧结工艺对Pa第二峰有影响,而Pa第二峰也影响烧结材料的微观结构.

There exist two Pa peaks of vacuum pressure when TiB2 is consolidated by Spark Plasma Sintering. The second Pa peak was investigated in this paper. The results indicate that it is caused by vapor deposition from chemical reaction in sintering. The state of original pow- der and sintering technology have influence on the second Pa peak which also has effect on the microstructure of the sintering materials.

参考文献

[1]
[2] Omori M, Okubo A, Gilhwan K, et al. J. Materials Synthesis &
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