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采用740℃热浸镀铝方法,在20碳钢表面制备热浸镀铝层.镀铝层经850℃扩散处理4 h后,采用SEM和XRD确定扩散层的相组成,采用TEM研究组成相的晶体学取向关系.分析AlFe3C0.5相的形成原因.结果表明:扩散层与基体之间存在Fe3Al、FeAl和点阵常数为0.377 nm的针叶状AlFe3C0.5相;针状AlFe3C0.5与Fe3Al相之间存在的晶体学取向关系是(220)Fe3Al//(-111)AlFe3C0.5、[1-10]Fe3Al//[-12-3]AlFe3C0.5.

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