采取中频加热和TSSG的方法,从掺入了6%(质量分数)K2O的同成分Li2O-Nb2O5熔体中生长出了近化学计量比铌酸锂单晶,其铁电畴结构为单畴结构,居里温度为1191.5℃.在此基础上,分别掺入0.05%(质量分数),0.16%(质量分数)和0.32%(质量分数)的氧化锰,生长了掺Mn近化学计量比的铌酸锂晶体,其铁电畴结构也均为单畴结构,居里温度分别为1195.3、1201.5和1219℃.对这4个晶体进行的红外光谱测试的结果表明:均在3466cm-1有一吸收峰.通过二波耦合实验,我们对不同掺杂浓度的4种晶体进行了光折变性能测试.
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