用高能球磨采用两种方案制备了FeCo+MnO体系,并用X射线衍射和振动样品磁强计对其结构和磁性质做了分析.发现采用直接氧化Mn而得到MnO的方法,所得体系的MnO较纯;而通过分解MnCO3得到MnO的体系,MnO纯度较低,有较多Mn3O4杂质,两种方法制备的FeCo+MnO体系的矫顽力和剩磁比都比单纯FeCo体系的增加很多,且前一种方法比后一种方法制备的FeCo+MnO体系的矫顽力和剩磁比较大.然后研究了球磨时间及退火处理对FeCo+MnO体系矫顽力及剩磁比的影响,发现球磨时间为120h体系的矫顽力和剩磁比最大;经过退火处理后,体系的矫顽力和剩磁比都有较大幅度的增加.
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