采用射频磁控溅射工艺，在（111）Pt／Ti／SiO2／Si衬底上用PZT（53／47）陶瓷靶制备铁电薄膜．用快速光热退火炉对原位沉积的薄膜进行RTA处理．薄膜的相结构由XRD确定．通过改变氩气和氧气的比例以及衬底温度，研究了溅射气氛和衬底温度对PZT铁电薄膜结构的影响．实验表明，在不同的溅射气氛和衬底温度条件下，薄膜会经历不同的相变过程．用RT66A标准铁电测试设备测量了薄膜的铁电性能，在外加电压为5V时，Pr=14.6μC／cm2，Ec＝82．gkV／cm．
PZT thin films were fabricated on (111)Pt/Ti/SiO2/Si by RF magnetron sputtering with a ceramic target(PZT53/47). The as-deposited
thin films were annealed with a rapid thermal annealing process. XRD was used to determine the structure of the thin films. This paper focused on the
research about the influence of sputtering gas and substrate temperature on the structure of the thin films. It was found that the process of phase
transformation of PZT thin films changed with the ratio of Ar to O2 and substrate temperatures. The ferroelectric property of PZT thin films
was measured by RT66A standardized ferroelectric test system. When 5V voltage was applied, the film showed a remnant polarization of 14.6μC/cm2, and coercive
field of 82.9kV/cm.
参考文献
| [1] | Araujo C A, McMillan L D, Melnic B M, et al. Ferroelectrics, 1990, 104: 241--256 2 Hwang Y S, Paek S H. J. Mater. Sci. Lett., 1995, 14 (5): 322--323 3 Okada A. J. Appl. Phys., 1978, 49 (8): 4495--4499 4 Hirata K, Hosokawa N, Hase T, et al. Jpn. J. Appl. Phys., Part 1, 1992, 31 (9B): 3021--3024 5 McClune W F. ed., Poder Diffraction File--Inorganic Volume (Int. Centre for Diffraction Data, Swarthmore,1986). File No. 25-447 6 McClune W F. ed., Poder Diffraction File--Inorganic Volume (Int. Centre for Diffraction Data, Swarthmore,1986). File No. 21-949 7 Aykan. J. Am. Ceram. Soc., 1968, 51(11-12): 577--581 8 Vasant Kumar C V R, Pascual R, Sayer M. J. Appl. Phys., 1992, 71 (2): 864--874 9 Iijima K, Ueda I, Kugimiya K. Jpn. J. Appl. Phys., Part 1, 1991, 30 (9B): 2149--2151 10 McClune W F. ed., Poder Diffraction File--Inorganic Volume (Int. Centre for Diffraction Data, Swarthmore,1986). File No. 26--142 |
- 下载量()
- 访问量()
- 您的评分：
-
10%
-
20%
-
30%
-
40%
-
50%