采用X 线衍射仪和EBSD分析研究近α型TA15钛合金在不同工艺参数下的热压缩变形组织和织构演变规律。结果表明:TA15合金热变形后淬火组织中存在针状马氏体α′相;晶粒在(101)和(002)滑移面上的滑移率先达到临界分切应力,发生塑性变形,使组织细化,并最终导致变形组织的择优取向;在小应变速率(0.01 s-1)和低变形温度(950℃)条件下,动态再结晶分数较高,产生较强的再结晶织构;随着变形温度和应变速率的升高,材料晶粒取向性减弱。
The microstructures and textures of TA15 titanium alloy after hot deformation under different process parameters were investigated by X-ray diffractometry (XRD) and electron back scattering diffractometry (EBSD). The results indicate that microstructures of TA15 alloy appear obvious acicular martensiteα′phase after hot deformation and quenching. The plastic deformation is going to occur in the slip systems of (101) and (002) slip planes by first reaching the critical resolved shear stress. The strong recrystallization textures are achieved at low deformation temperature and low strain rate, which will be weakened with increasing the strain rate and temperature.
参考文献
[1] | 李萍,段园培,薛克敏,王晓溪,甘国强.TB8钛合金的热变形组织与织构[J].中国有色金属学报,2010(05):872-877. |
[2] | 段园培 .TB8合金热变形组织介观尺度研究与模拟[D].合肥工业大学,2009. |
[3] | Effect of hydrogen on fracture behavior of Ti-6Al-4V alloy by in-situ tensile test[J].International journal of hydrogen energy,2010(4):p.1829. |
[4] | 袁宝国,于海平,李春峰.氢含量对Ti-6Al-4V合金室温高速压缩性能的影响[J].中国有色金属学报(英文版),2012(12):2943-2951. |
[5] | 陈强.合金加工流变学及其应用[M].北京:冶金工业出版社,2012 |
[6] | Glavicic MG;Kobryn PA;Semiatin SL .Validation of an automated EBSD method to deduce the beta-phase texture in Ti-6Al-4V with a colony-alpha microstructure[J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,2004(1/2):372-376. |
[7] | Zaefferer S. .A study of active deformation systems in titanium alloys: dependence on alloy composition and correlation with deformation texture[J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,2003(1/2):20-30. |
[8] | M. G. Glavicic;A. A. Salem;S. L. Semiatin .X-ray line-broadening analysis of deformation mechanisms during rolling of commercial-purity titanium[J].Acta materialia,2004(3):647-655. |
[9] | M.G. Glavicic;S.L. Semiatin .X-ray line-broadening investigation of deformation during hot rolling of Ti-6Al-4V with a colony-alpha microstructure[J].Acta materialia,2006(20):5337-5347. |
[10] | SEWARD G G E;CELOTTO S;PRIOR D J;WHEELER J POND R C .In situ SEM-EBSD observations of the hcp to bcc phase transformation in commercially pure titanium[J].Acta Materialia,2004,52(04):821-832. |
[11] | J.V. BERNIER;J.-S. PARK;A.L. PILCHAK .Measuring Stress Distributions in Ti-6Al-4V Using Synchrotron X-Ray Diffraction[J].Metallurgical and materials transactions. A, physical metallurgy and materials science,2008(13):3120-3133. |
[12] | 曾柯,辛仁龙,李波,汪炳叔,黄光杰,刘庆.EBSD技术在稀土变形镁合金微观表征中的应用[J].电子显微学报,2010(01):59-62. |
[13] | 杨平,孙祖庆,毛卫民.取向成像:一种有效研究晶体材料组织、结构及取向的技术[J].中国体视学与图像分析,2001(01):50-54,32. |
[14] | Glavicic MG.;Kobryn PA.;Spadafora F.;Semiatin SL. .Texture evolution in vacuum arc remelted ingots of Ti-6Al-4V[J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,2003(1/2):8-18. |
[15] | Glavicic MG.;Kobryn PA.;Bieler TR.;Semiatin SL. .An automated method to determine the orientation of the high-temperature beta phase from measured EBSD data for the low-temperature alpha-phase in Ti-6Al-4V[J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,2003(1/2):258-264. |
[16] | M.G. Glavicic;J.D. Miller;S.L. Semiatin .A Method to Measure the Texture of Secondary Alpha in Bimodal Titanium-Alloy Microstructures[J].Scripta materialia,2006(2):281-286. |
[17] | 李秀莲,王茂银,辛仁龙,黄光杰,刘庆.AZ31镁合金挤压轧制过程微观织构演变[J].材料热处理学报,2010(05):61-64. |
[18] | 邓运来,张新明,刘瑛,唐建国,周卓平.冷轧高纯铝柱状晶粒的组织与微取向的不均匀性[J].中国有色金属学报,2005(08):1173-1178. |
[19] | 曹鹏,方刚,雷丽萍,曾攀.多晶铜压缩过程中晶粒取向演化的塑性理论分析[J].金属学报,2007(09):913-919. |
[20] | 李成铭,李萍,赵蒙,薛克敏.TA15钛合金高温压缩变形行为与组织研究[J].航空材料学报,2013(03):25-29. |
[21] | 赵永庆;陈永楠;张学敏;曾卫东 王磊.钛合金相变及热处理[M].长沙:中南大学出版社,2012 |
[22] | Weiss, I;Semiatin, SL .Thermomechanical processing of alpha titanium alloys--an overview[J].Materials Science & Engineering. A, Structural Materials: Properties, Microstructure and Processing,1999(2):243-256. |
[23] | 朱知寿,王新南,童路,刘东升.新型TC21钛合金相变行为和相组成研究[J].稀有金属快报,2006(12):23-27. |
[24] | Run Huang;Yong Han.Structure evolution and thermal stability of SMAT-derived nanograined layer on Ti-25Nb-3Mo-3Zr-2Sn alloy at elevated temperatures[J].Journal of Alloys and Compounds: An Interdisciplinary Journal of Materials Science and Solid-state Chemistry and Physics,2013:1-11. |
[25] | P. Wanjara;M. Jahazi;H. Monajati;S. Yue .Influence of thermomechanical processing on microstructural evolution in near-α alloy IMI834[J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,2006(1/2):300-311. |
- 下载量()
- 访问量()
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%