Nanocrystal carbonated hydroxyapatite was prepared by lecithin-controlled chemical precipitation in synthetic body fluid (SBF). The reactant was aged and heated at 850 ℃ for crystallization. The morphology and microstructure of the carbonated hydroxyapatite were investigated using transmission electron microscope( TEM ), X- rey diffraction (XRD) and FTIR. The experimental results demonstrate that the shapes of earbonated hydroxyapatite particles display spheres with the average size of 20- 28 nm, and carbonated hydroxyapatite contained carbonate ions, similar to mineral of bone tissues.
参考文献
[1] | Larry L. Hench .Bioceramics[J].Journal of the American Ceramic Society,1998(7):1705-1728. |
[2] | Yeon KC;Wang J;Ng SC .Mechanochemical synthesis of nanocrystalline hydroxyapatite from CaO and CaHPO4.[J].Biomaterials,2001(20):2705-2712. |
[3] | Rhee SH .Synthesis of hydroxyapatite via mechanochemical treatment.[J].Biomaterials,2002(4):1147-1152. |
[4] | Liu DM;Troczynski T;Tseng WJ .Aging effect on the phase evolution of water-based sol-gel hydroxyapatite.[J].Biomaterials,2002(4):1227-1236. |
[5] | Tadic D;Peters F;Epple M .Continuous synthesis of amorphous carbonated apatites.[J].Biomaterials,2002(12):2553-2559. |
[6] | Li Y;Li YD;Deng ZX;Zhuang J Sun XM .Surfactant-assistanted Hydrothermal Synthesis of Hydroxyapatite Nanorods[J].International Journal of Inorganic Materials,2001,3:633-637. |
[7] | Wantae Kim;Fumio Saito .Sonochemical synthesis of hydroxyapatite from H_(3)PO_(4) solution with Ca(OH)_(2)[J].Ultrasonics,2001(2):85-88. |
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