利用高能球磨,通过剧烈的塑性变形,使Fe、AI粉末颗粒发生细化和机械合金化,并产生高的畸变能和界面能,在560℃和620℃进行低温烧结,Fe、Al原子沿着大量的晶界和缺陷进行扩散,形成FeAl合金相.经过12h的高能球磨.620℃烧结、保温4h,可以使Fe、Al复合粉完全转变成FeAl金属间化合物.晶粒均匀细小,呈现等轴状,晶粒大小约为30nm.
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