Three-dimensional atom probe (3DAP) technique has been used to study the nucleation and growth of M23C6 carbide in a supersaturated multi-component Fe-based alloy aged at 800℃. 3D images indicate that the radius of M23C6 carbide after ageing for 10 min is about 9 nm. Concentration profiles of alloy elements in the carbide are also obtained. Combined with PANDAT and Thermo-Calc software, attempts to model the early stages of precipitation are present. The calculated particle size and composition of M23C6 carbide is in good agreement with 3DAP data.
参考文献
[1] | M.K. Miller;R.G. Forbes .Atom probe tomography[J].Materials Characterization,2009(6):461-469. |
[2] | D. H. Ping;M. Ohnuma;Y. Hirakawa .Microstructural evolution in 13Cr-8Ni-2.5Mo-2Al martensitic precipitation-hardened stainless steel[J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,2005(1/2):285-295. |
[3] | Y.Y. Song;D.H. Ping;F.X. Yin;X.Y. Li;Y.Y. Li .Microstructural evolution and low temperature impact toughness of aFeC13%CrC4%NiCMo martensitic stainless steel[J].Materials Science & Engineering. A, Structural Materials: Properties, Misrostructure and Processing,2010(3):614-618. |
[4] | W. Cao;S.-L. Chen;F. Zhang;K. Wu;Y. Yang;Y.A. Chang;R. Schmid-Fetzer;W.A. Oates .PANDAT software with PanEngine, PanOptimizer and PanPrecipitation for multi-component phase diagram calculation and materials property simulation[J].Calphad: Computer Coupling of Phase Diagrams and Thermochemistry,2009(2):328-342. |
[5] | J. D. Robson .Modelling the evolution of particle size distribution during nucleation, growth and coarsening[J].Materials Science and Technology: MST: A publication of the Institute of Metals,2004(4):441-448. |
[6] | J. Y. Xie;N. X. Chen;L. D. Teng .Atomistic study on the site preference and thermodynamic properties for Cr_(23-x)Fe_AC_6[J].Acta materialia,2005(20):5305-5312. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%