分别通过超声共混法和原位还原法制备了石墨烯/环氧树脂复合材料.利用X射线光电子能谱(XPS)、X射线衍射(XRD)、光学显微镜和扫描电子显微镜(SEM)对复合材料的结构进行了表征,并对其力学性能进行了测试.结果表明,原位还原法制备的石墨烯/环氧树脂复合材料中,氧化石墨烯已经被成功地还原为石墨烯,并且石墨烯具有良好的分散性.力学性能测试结果表明,两种方法制备的复合材料的力学强度较纯环氧树脂明显提高.当石墨烯的量为m(GO)/m (EP)=0.3/100时,超声混合法制备的石墨烯/环氧树脂复合材料的拉伸强度和弯曲强度分别最大提高约29.2％和1.4％；而原位还原法制备的石墨烯/环氧树脂复合材料的拉伸强度和弯曲强度分别最大提高约40.5％和9.4％.
参考文献
| [1] | Compton, OC;Nguyen, ST .Graphene Oxide, Highly Reduced Graphene Oxide, and Graphene: Versatile Building Blocks for Carbon-Based Materials[J].Small,2010(6):711-723. |
| [2] | Horacio Javier Salavagione;Gerardo Martinez;Marian A. Gomez .Synthesis of poly(vinyl alcohol)/reduced graphite oxide nanocomposites with improved thermal and electrical properties[J].Journal of Materials Chemistry: An Interdisciplinary Journal dealing with Synthesis, Structures, Properties and Applications of Materials, Particulary Those Associated with Advanced Technology,2009(28):5027-5032. |
| [3] | Yang, X.;Li, L.;Shang, S.;Tao, X.-M. .Synthesis and characterization of layer-aligned poly(vinyl alcohol)/graphene nanocomposites[J].Polymer: The International Journal for the Science and Technology of Polymers,2010(15):3431-3435. |
| [4] | Song, P.;Cao, Z.;Cai, Y.;Zhao, L.;Fang, Z.;Fu, S. .Fabrication of exfoliated graphene-based polypropylene nanocomposites with enhanced mechanical and thermal properties[J].Polymer: The International Journal for the Science and Technology of Polymers,2011(18):4001-4010. |
| [5] | Sasha Stankovich;Richard D.Piner;Xinqi Chen;Nianqiang Wu;SonBinh T.Nguyen;Rodney S.Ruoff .Stable aqueous dispersions of graphitic nanoplatelets via the reduction of exfoliated graphite oxide in the presence of poly(sodium 4-styrenesulfonate)[J].Journal of Materials Chemistry: An Interdisciplinary Journal dealing with Synthesis, Structures, Properties and Applications of Materials, Particulary Those Associated with Advanced Technology,2006(2):155-158. |
| [6] | Jiali Zhang;Haijun Yang;Guangxia Shen;Ping Cheng;Jingyan Zhang;Shouwu Guo .Reduction of graphene oxide via L-ascorbic acid[J].Chemical communications,2010(7):1112-1114. |
| [7] | Shin-Yi Yang;Wei-Ning Lin;Yuan-Li Huang .Synergetic effects of graphene platelets and carbon nanotubes on the mechanical and thermal properties of epoxy composites[J].Carbon: An International Journal Sponsored by the American Carbon Society,2011(3):793-803. |
| [8] | Jiajie Liang;Yi Huang;Long Zhang;Yan Wang;Yanfeng Ma;Tianyin Guo;Yongsheng Chen .Molecular-Level Dispersion of Graphene into Poly(vinyl alcohol) and Effective Reinforcement of their Nanocomposites[J].Advanced functional materials,2009(14):2297-2302. |
| [9] | Zaman, I.;Phan, T.T.;Kuan, H.-C.;Meng, Q.;Bao La, L.T.;Luong, L.;Youssf, O.;Ma, J. .Epoxy/graphene platelets nanocomposites with two levels of interface strength[J].Polymer: The International Journal for the Science and Technology of Polymers,2011(7):1603-1611. |
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