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采用硅作为熔渗剂,利用真空反应烧结的工艺,在1600℃烧结制得了结构致密、密度低的碳化硅-氮化铝(SiC/AlN)复合材料,分析测试了所制得的复合材料的物相、微观结构和力学性能.结果表明,氮化铝的添加量由2wt%增加到10wt%时,复合材料的力学性能出现先增加后减小的趋势,当AlN含量为6wt%时,得到复合材料的力学性能最高,其抗弯强度为256 MPa,显微硬度为2660 HV.加入AlN后,复合材料的孔隙率略微有点上升,烧结体的密度在2.95 ~3.01 g/cm3之间.复合材料的主要组成相为SiC、AlN和Si.

参考文献

[1] Zhang, Chi;Yao, Xiumin;Li, Yinsheng;Lian, Hanqin;Chen, Jian;Zhang, Jingxian;Yang, Jian;Li, Xiaoyun;Qiu, Tai;Chen, Zhongming;Liu, Xuejian;Huang, Zhengren.Effect of AlN addition on the thermal conductivity of pressureless sintered SiC ceramics[J].CERAMICS INTERNATIONAL,20157(7):9107-9114.
[2] Xiaoming Duan;Dechang Jia;Biao Yuan.Effect of solid contents on the mechanical properties of SiC~10 wt.%AlN ceramic composites prepared by gelcasting[J].Journal of Alloys and Compounds: An Interdisciplinary Journal of Materials Science and Solid-state Chemistry and Physics,2013:275-279.
[3] Haiyang Zhao;Weimin Wang;Zhengyi Fu.Thermal conductivity and dielectric property of hot-pressing sintered A1N-BN ceramic composites[J].CERAMICS INTERNATIONAL,20091(1):105-109.
[4] Y.Pan and D.Jiang.SiC-AlN particulate composite[J].Journal of the European Ceramic Society,19999(9):1789-1793.
[5] Kim, Kwang Joo;Kim, Young-Wook;Lim, Kwang-Young;Nishimura, Toshiyuki;Narimatsu, Eiichirou.Electrical and thermal properties of SiC-AlN ceramics without sintering additives[J].Journal of the European Ceramic Society,201510(10):2715-2721.
[6] Daoush, W.;Francis, A.;Lin, Y.;German, R..An exploratory investigation on the in-situ synthesis of SiC/AlN/Al composites by spark plasma sintering[J].Journal of Alloys and Compounds: An Interdisciplinary Journal of Materials Science and Solid-state Chemistry and Physics,2015:458-462.
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