不锈钢基PbO2-WC—CeO2复合电极克服了传统钛基二氧化铅（DSA）电极基体易钝化、寿命短和成本高等缺点，以往对其电化学性能研究不多。采用复合电沉积方式在不锈钢基体上制备了PbO2-WC—CeO2复合电极，通过循环伏安曲线（CV）考察了复合电极的电沉积过程；通过x射线衍射（XRD）、能谱分析仪考察了复合电极的元素组成；通过扫描电镜（SEM）考察了复合电极的表面形貌变化；通过Talel曲线、析氧曲线考察了电极掺杂前后的电化学性能变化。结果表明：wc和CeO2固体颗粒的加入使得PbO2电沉积过程发生了择优生长和晶粒细化，电极耐腐蚀性能提高，催化活性和节能性能变佳。
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