用磁控溅射法将NiTi薄膜沉积在纯Cu箔片上,在800℃分别固溶30 min,45 min,60min和120 min;采用X射线傅氏线形分析法计算各固溶时间的位错密度及位错分布参量.随固溶时间的增加,平均位错密度不断下降;亚晶粒尺寸D逐渐增加;平均位错分布参量基本不变.由位错密度及位错分布参量计算得到NiTi薄膜材料的显微硬度值,随固溶时间的增加,显微硬度计算值明显低于测量值.
参考文献
[1] | 梁芳慧,周廉.钛和钛合金生物活化研究现状[J].稀有金属材料与工程,2003(04):241-245. |
[2] | 岳珠峰,万建松,张庆茂.一种形状记忆合金的本构模型及其应用[J].稀有金属材料与工程,2003(04):246-249. |
[3] | M. Kohl;D. Dittmann;E. Quandt;B. Winzek;S. Miyazaki;D. M. Allen .Shape memory microvalves based on thin films or rolled sheets[J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,1999(0):784-788. |
[4] | 张新平,于思荣,夏连杰,何镇明.钛及钛合金在牙科领域中的研究现状[J].稀有金属材料与工程,2002(04):246-251. |
[5] | 梁成浩,隋洪艳.TiNiCu形状记忆合金的耐蚀性研究[J].稀有金属材料与工程,2001(02):93-96. |
[6] | Ken K. Ho;Gregory P. Carman .Sputter deposition of NiTi thin film shape memory alloy using a heated target[J].Thin Solid Films: An International Journal on the Science and Technology of Thin and Thick Films,2000(1/2):18-29. |
[7] | Busch J D;Lee C H .Shape-Memory Properties in Ni-Ti Sputter-Deposited Film[J].Journal of Applied Physics,1990,68:6224-6228. |
[8] | Nishida M;Wayman C M .Precipitation Processes in NearEquiatomic TiNi Shape Memory Alloys[J].Metallurgical and Materials Transactions,1986,17:1505. |
[9] | POROD G .Die Rontgenkleinwinkelstreung Von Dichtgepackten Kolloiden Systemen[J].Kolloidnyi Zhurnal,1951,124:83-114. |
[10] | MENG F L;Chai Z G;Wang Y M .Small-Angle X-ray Scattering Study of the δ' Phase Growth Kinetic in 1420Al-Li Alloy[J].Materials Characterization,2001,47:43-46. |
[11] | 柴志刚,孟繁玲,邹青,王煜明.Small-angle x-ray scattering study of the formation and growth of δ′in binary Al-7.87at% Li alloy[J].中国物理(英文版),2002(02):191-193. |
[12] | 孟繁玲,李永华,徐耀,王煜明.小角x射线散射确定TiNi薄膜中晶化粒子的长大激活能[J].物理学报,2002(09):2086-2089. |
[13] | Wang Y;Lee S;Lee Y .X-ray Line Profile Analysis of Deformed Al[J].Journal of Applied Crystallography,1982,15:35-38. |
[14] | Warren B E.X-ray Diffraction[M].London:Addsion Wesley Press,1968:105-115. |
[15] | Zhang N;Wang Y .Dislocation and Hardness of Hard Coatings[J].THIN SOLID FILMS,1992,214:4-5. |
[16] | 单凤兰,霍艳玲,滕凤恩.TiNi形状记忆合金薄膜的位错与相变[J].稀有金属材料与工程,1998(04):199-201. |
[17] | F. L. Shan;Z. M. Gao;Y. M. Wang .Microhardness evaluation of Cu-Ni multilayered films by X-ray diffraction line profile analysis[J].Thin Solid Films: An International Journal on the Science and Technology of Thin and Thick Films,1998(1/2):162-164. |
[18] | 李永华,纪红,孟繁玲,邱利霞,郑伟涛,王煜明.衬底温度对沉积的NiTi薄膜晶化行为的影响[J].材料科学与工艺,2003(03):251-253. |
[19] | Yang Y Q;Jia H S;Zhang Z F et al.Transformation in Sputter-deposited Thin Films of NiTi Shape Memory Alloy[J].Materials Letters,1995,22:137-140. |
[20] | Li B;Rong L et al.Fabrication of Cellular NiTi Intermetallic Compounds[J].Journal of Materials Research,2000,15:10-13. |
[21] | Ishida A;Sato M;Takei A et al.Effect of Aging on Shape Memory Behavior of Ti-51.3 at% Ni Thin Films[J].Metallurgical and Materials Transactions A:Physical Metallurgy and Materials Science,1996,27:3753-3759. |
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