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以鳞片石墨为原料,采用Hummers法制备氧化石墨.氧化石墨与硝酸银溶液混合超声处理,通过功能离子预吸附的方式,将银离子有效地分散在氧化石墨烯载体上.以水合肼为还原剂,同时还原氧化石墨和硝酸银溶液中的银离子,原位制备银-石墨烯复合材料.采用X射线衍射仪、扫描电子显微镜对制得的银-石墨烯复合材料进行表征,并对复合材料的电化学性能进行分析.结果显示,制得银-石墨烯复合材料的比电容明显高于单纯的石墨烯材料,电化学性质优异,是理想的电化学电容器电极材料.

参考文献

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[5] 傅玲,邹艳红,刘洪波,何月德.氧化石墨及其聚合物纳米复合材料的研究现状[J].炭素技术,2005(02):21-26.
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[7] 雷芸,张科,潘群,邹琴,袁继祖.石墨烯载钴材料的制备[J].硅酸盐通报,2011(01):98-100.
[8] 雷芸,江莹,钱坤,何静,陈禹成.石墨烯/TiO2复合材料的制备及其光催化性能的研究[J].硅酸盐通报,2012(02):243-246.
[9] 邹正光,俞惠江,龙飞,范艳煌.超声辅助Hummers法制备氧化石墨烯[J].无机化学学报,2011(09):1753-1757.
[10] Ong, B.K.;Poh, H.L.;Chua, C.K.;Pumera, M. .Graphenes Prepared by Hummers, Staudenmaier and Hofmann Methods for Analysis of TNT-Based Nitroaromatic Explosives in Seawater[J].Electroanalysis,2012(11):2085-2093.
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