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采用载波钝化方法对AZ91D镁合金进行载波钝化,使用原子力显微镜(AFM)、接触角仪(FTA)仪器和X射线光电子谱仪(XPS)研究了载波钝化对AZ91D镁合金表面特性的影响。结果表明:载波钝化后AZ91D镁合金表面生成一层均匀且致密的表面膜,内层由 MgO和少量Al2O3组成,外层由Mg(OH)2、MgO和少量 Al(OH)3组成。

AZ91D magnesium alloy was treated by alternating voltage (AV) modulated passivation technique. Atomic force microscopy (AFM), First ten angstroms (FTA) contact angle-meter and X-ray photoelectron spectroscopy (XPS) were employed to investigate the influence of AV-modulated passivation on the surface properties of the films formed on the AZ91D magnesium alloy after AV-modulated passivation. The results showed that a uniform and stable film was formed after AV-modulated passivation. The surface films on the samples after AV-modulated passivation consist of an inner layer rich in MgO, with a little Al2O3,and an outer layer of Mg(OH)2,MgO with a little Al(OH)3.

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