报道了用反滴定共沉淀法及低温煅烧前驱体的方法制备Ce3+摻杂的Lu3Al5O12石榴石陶瓷发光粉体的研究. 通过对实验中制备的Lu3Al5O12∶ Ce前驱体和煅烧粉体进行的X射线粉末衍射(XRD)和透射电镜(TEM)的测试表征表明, 在1000 ℃烧结热处理2 h即可获得完全单一的立方相Lu3Al5O12∶ Ce粉体, 粉体的平均粒径～30 nm. 而随烧结温度的增加, 粒径有增大的趋势. 在1000 ℃空气氛热处理的Lu3Al5O12∶ 0.5%Ce发光粉体具有最强的荧光发射. 粉体经干压、等静压成型后, 在1800 ℃经流动的H2气氛常压烧结保温6 h可获得半透明Lu3Al5O12∶ 0.5%Ce陶瓷. X射线激发下的快分量衰减时间短至十几ns, 占发光成分中主要部分的慢分量为～100 ns.
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