采用普通球磨细化工艺和两次球磨细化工艺制备出两类Al2O3/ZrB2/ZrO2复合陶瓷材料,并对材料的硬度、断裂韧性和抗弯强度进行了测试和分析.结果表明,两次球磨细化工艺可以明显降低ZrB2/ZrO2晶粒的尺寸至0.2~0.4μm,使其在Al2O3基体内的分布更均匀,并能有抑制Al2O3晶粒的异常长大.与普通细化工艺相比较,此工艺改变了材料的断裂模式,强化了晶界的结合能力,使复合材料的综合力学性能得到了更大程度的改善,其中抗弯强度和硬度最多提高了48%和41%.
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