采用一种新颖的微波水热法制备VO2粉体,利用扫描电镜(SEM)表征所合成粉体的微观形貌,调节H2O2的浓度、微波功率、微波时间、pH值、水热反应时间及钨掺杂剂等合成工艺参数,实现了对VO2粉体形貌的调控.结果表明:控制不同的工艺参数可合成具有不同形貌如球形、空心椭球形,花簇状、棒状等VO2粉体.
参考文献
| [1] | LIANG Jiran,HI Ming,KAN Qiang,LIANG Xiuqin,WANG Xiaodong,LI Guike,CHEN Hongda.Infrared transition properties of vanadium dioxide thin films across semiconductor-metal transition[J].稀有金属（英文版）,2011(03):247-251. |
| [2] | Lopez R;Haglund RF;Feldman LC;Boatner LA;Haynes TE .Optical nonlinearities in VO2 nanoparticles and thin films[J].Applied physics letters,2004(22):5191-5193. |
| [3] | Yan Jiazhen;Zhang Yue;Huang Wanxia;Tu Mingjin .Effect Of Mo-w Co-doping On Semiconductor-metal Phase Transition Temperature Of Vanadium Dioxide Film[J].Thin Solid Films: An International Journal on the Science and Technology of Thin and Thick Films,2008(23):8554-8558. |
| [4] | Burkhardt W.;Christmann T.;Franke S.;Kriegseis W.;Meister D.;Meyer BK.;Niessner W.;Schalch D.;Scharmann A. .Tungsten and fluorine co-doping of VO2 films[J].Thin Solid Films: An International Journal on the Science and Technology of Thin and Thick Films,2002(1/2):226-231. |
| [5] | Pragna Kiri;Michael E.A. Warwick;Ian Ridley;Russell Binions .Fluorine doped vanadium dioxide thin films for smart windows[J].Thin Solid Films: An International Journal on the Science and Technology of Thin and Thick Films,2011(4):1363-1366. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分：
-
10%
-
20%
-
30%
-
40%
-
50%